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TO-15 Canister Relative Humidity: Part IIIb (Humidifying Your Sample… My Preferred Approach)

29 Oct 2013

So let us recap this multi-blog series on relative humidity (RH):

Part I –  We learn what is RH and why do we care about it when sampling/analyzing whole air canister samples for volatile organic compounds (VOCs).

Part II – We learn how to calculate the theoretical % RH in a canister.

Part IIIa – We learn how to generate a humidified blank by direct injection of DI water.

Now… time for me to show you (in the following VIDEO) how I prefer to humidify my blanks and standards with the use of our humidification chamber (catalog # 24282) and vacuum/pressure gauge (catalog # 24285):

One very important part I left out on the video: Be very careful if you are relying on your dynamic diluter to generate your humidified blanks and/or standards. Some diluters do not even come equipped with a humidification chamber. While other diluters have a humidification chamber; however, the effluent gas stream may not be reaching the RH levels you are trying to achieve. For example: One customer was shocked to see that their gas stream was only reaching 18% RH @ a 1 L/min flow rate and only 12% RH @ a 5 L/min flow rate (see picture below… you should recognize my equilibration chamber and Extech hygrometer). Now… 18% RH may not be that bad… if your samples are coming from the Gobi Desert. However, if you want to obtain higher RH levels with such a diluter you will need to supplement your blanks/standards with a direct shot of DI (as shown in Part IIIa) prior to hooking up to your diluter.

blog to 15 canister relative humidity part iiib humidifying your sample. my preferred approach 01

Stay tuned for part IV where I finally show you why I am making such a big deal about RH!

Products Mentioned


Camera di umidificazione
Manometro di prova analogico Ashcroft, diametro 6", NPT 1/4", da 30” Hg a 60 psi

Author

  • Jason Herrington, PhD

    Jason joined Restek in 2011 after spending over 10 years in environmental analysis, most notably as a postdoctoral research fellow with the U.S. EPA focusing on the development of techniques for organic speciation of ambient gas-phase and particulate air toxics. He has a BS in environmental sciences from Rutgers University and a PhD in exposure science from The University of Medicine and Dentistry of New Jersey. His wide-ranging work has been published in over a dozen peer-reviewed manuscripts and presented around the world. As a senior scientist with Restek, Jason is heavily involved with developing new air products and applications.

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