{"id":43421,"date":"2020-10-21T00:00:00","date_gmt":"2020-10-21T00:00:00","guid":{"rendered":"https:\/\/discover.restek.com\/uncategorized\/japanese-pfas-lc-column-anatomy-which-phase-dimensions-and-particle-type-are-best\/"},"modified":"2026-04-15T16:40:40","modified_gmt":"2026-04-15T16:40:40","slug":"japanese-pfas-lc-column-anatomy-which-phase-dimensions-and-particle-type-are-best","status":"publish","type":"post","link":"https:\/\/discover.restek.com\/ja\/articles-ja\/evar3069-ja\/japanese-pfas-lc-column-anatomy-which-phase-dimensions-and-particle-type-are-best","title":{"rendered":"PFAS\u5206\u6790\u7528\u306eLC \u30ab\u30e9\u30e0\u306b\u306f\u3001\u3069\u306e\u56fa\u5b9a\u76f8\u3001\u30b5\u30a4\u30ba\u3001\u7c92\u5b50\u5f84\u304c\u6700\u9069\u304b\uff1f"},"content":{"rendered":"\n

\u30d1\u30fc\u30d5\u30eb\u30aa\u30ed\u304a\u3088\u3073\u30dd\u30ea\u30d5\u30eb\u30aa\u30ed\u30a2\u30eb\u30ad\u30eb\u5316\u5408\u7269(PFAS)\u306e\u30b5\u30f3\u30d7\u30eb\u3092\u65e5\u5e38\u7684\u306b\u691c\u67fb\u3057\u3066\u3044\u308b\u591a\u304f\u306e\u30e9\u30dc\u3067\u306f\u3001\u3053\u308c\u3089\u300c\u6c38\u9060\u306e\u5316\u5b66\u7269\u8cea\u300d\u306e\u62e1\u6563\u3084\u6b8b\u7559\u6027\u3001\u6f5c\u5728\u7684\u306a\u5065\u5eb7\u30ea\u30b9\u30af\u304c\u3088\u308a\u7406\u89e3\u3055\u308c\u308b\u306b\u3064\u308c\u3066\u3001\u8a8d\u77e5\u5ea6\u3084\u95a2\u5fc3\u304c\u9ad8\u307e\u3063\u3066\u3044\u308b\u3053\u3068\u306f\u3054\u5b58\u3058\u3067\u3057\u3087\u3046\u3002\u95a2\u5fc3\u304c\u9ad8\u307e\u308b\u306b\u3064\u308c\u3066\u3001\u8fc5\u901f\u3001\u6b63\u78ba\u3001\u7cbe\u5ea6\u306e\u826f\u3044\u691c\u67fb\u306e\u5fc5\u8981\u6027\u304c\u5897\u3057\u3066\u3044\u307e\u3059\u3002\u3053\u306e\u3088\u3046\u306a\u9700\u8981\u306f\u3001\u3088\u308a\u826f\u3044\u30e1\u30bd\u30c3\u30c9\u306e\u958b\u767a\u3092\u4fc3\u3057\u3066\u304a\u308a\u3001LC\u30ab\u30e9\u30e0\u306e\u9078\u629e\u306f\u3001\u6539\u5584\u3055\u308c\u305f\u30a2\u30d7\u30ed\u30fc\u30c1\u3092\u69cb\u7bc9\u3059\u308b\u305f\u3081\u306e\u8981\u3067\u3059\u3002\u3053\u308c\u306f\u3001\u76e3\u8996\u3055\u308c\u308bPFAS\u306e\u30ea\u30b9\u30c8\u304c\u3001\u307e\u3059\u307e\u3059\u77ed\u3044\u30a2\u30eb\u30ad\u30eb\u9396\u5316\u5408\u7269\u3092\u542b\u3080\u3088\u3046\u306b\u306a\u308b\u306b\u3064\u308c\u3001\u7279\u306b\u91cd\u8981\u306b\u306a\u308a\u307e\u3059\u3002\u3053\u3053\u3067\u306f\u3001PFAS\u5206\u6790\u306e\u305f\u3081\u306eLC\u30ab\u30e9\u30e0\u3092\u9078\u629e\u3059\u308b\u969b\u306b\u8003\u616e\u3059\u3079\u304d\u91cd\u8981\u306a\u7279\u6027\u3092\u691c\u8a0e\u3057\u307e\u3059\u3002<\/p>\n\n\n\n

\u30ab\u30e9\u30e0\u56fa\u5b9a\u76f8\u3068\u30b5\u30a4\u30ba\u306e\u9078\u629e<\/h2>\n\n\n\n

\u3069\u306ePFAS LC\u30ab\u30e9\u30e0\u3092\u4f7f\u7528\u3059\u308b\u304b\u3092\u6c7a\u5b9a\u3059\u308b\u969b\u306b\u306f\u3001\u307e\u305a\u306f\u6709\u52b9\u306a\u56fa\u5b9a\u76f8\u3092\u7279\u5b9a\u3059\u308b\u5fc5\u8981\u304c\u3042\u308a\u307e\u3059\u3002\u3053\u306e\u7279\u5b9a\u306b\u306f\u3001\u3069\u306e\u7bc4\u56f2\u306ePFAS\u3092\u5bfe\u8c61\u3068\u3059\u308b\u304b\u304c\u91cd\u8981\u3067\u3059\u3002<\/p>\n\n\n\n

\u8d85\u77ed\u9396\uff5e\u9577\u9396PFAS\u3092\u5305\u62ec\u7684\u306b\u8a55\u4fa1\u3059\u308b\u306a\u3089Ultra IBD Inert<\/h2>\n\n\n\n

\u5e83\u7bc4\u56f2\u306aPFAS\u6c5a\u67d3\u306e\u5b9f\u614b\u3092\u5305\u62ec\u7684\u306b\u8a55\u4fa1\u3059\u308b\u305f\u3081\u306b\u306f\u3001\u6c34\u4e2d\u306b\u542b\u307e\u308c\u308b\u8d85\u77ed\u9396\u304b\u3089\u9577\u9396\u307e\u3067\u306ePFAS\u3092\u540c\u6642\u306b\u5206\u6790\u3067\u304d\u308b\u624b\u6cd5\u304c\u4e0d\u53ef\u6b20\u3067\u3059\u3002\u5f93\u6765\u3001\u6c34\u4e2d\u306e\u77ed\u9396PFAS\uff08C4\u4ee5\u4e0a\uff09<\/strong>\u306e\u5206\u6790\u306b\u306f\u3001\u9006\u76f8\u6db2\u4f53\u30af\u30ed\u30de\u30c8\u30b0\u30e9\u30d5\u30a3\u30fc\uff08RPLC\uff09\u3084C18\u30ab\u30e9\u30e0\u3092\u4f7f\u7528\u3057\u305f\u30e1\u30bd\u30c3\u30c9\u304c\u5e83\u304f\u7528\u3044\u3089\u308c\u3066\u304d\u307e\u3057\u305f\u3002\u3057\u304b\u3057\u3001\u3053\u308c\u3089\u306e\u30e1\u30bd\u30c3\u30c9\u3067\u306f\u3001\u6975\u6027\u306e\u9ad8\u3044\u8d85\u77ed\u9396PFAS<\/strong>\u3001\u7279\u306b\u30c8\u30ea\u30d5\u30eb\u30aa\u30ed\u9162\u9178\uff08TFA\uff09\u306a\u3069\u3092\u5341\u5206\u306b\u4fdd\u6301\u3059\u308b\u3053\u3068\u304c\u96e3\u3057\u304f\u3001\u30de\u30c8\u30ea\u30c3\u30af\u30b9\u7531\u6765\u306e\u5e72\u6e09\u304b\u3089\u306e\u5206\u96e2\u3082\u56f0\u96e3\u3067\u3042\u308b\u3068\u3044\u3046\u8ab2\u984c\u304c\u3042\u308a\u307e\u3059\u3002\u3053\u306e\u8ab2\u984c\u306b\u5bfe\u51e6\u3059\u308b\u305f\u3081\u3001\u30cf\u30a4\u30d6\u30ea\u30c3\u30c9HILIC\u304a\u3088\u3073\u30a4\u30aa\u30f3\u4ea4\u63dbLC\u30ab\u30e9\u30e0\u3092\u7528\u3044\u305f\u3001\u6c34\u30b5\u30f3\u30d7\u30eb\u4e2d\u306e\u8d85\u77ed\u9396\u304a\u3088\u3073\u77ed\u9396PFAS<\/strong>\u306b\u7279\u5316\u3057\u305f\u8fc5\u901f\u5206\u6790\u30e1\u30bd\u30c3\u30c9\u304c\u958b\u767a\u3055\u308c\u307e\u3057\u305f\u3002\u305f\u3060\u3057\u3001\u3053\u306e\u30e1\u30bd\u30c3\u30c9\u306f\u9577\u9396PFAS<\/strong>\u306f\u5bfe\u8c61\u5916\u3067\u3042\u308b\u305f\u3081\u3001PFAS\u5168\u4f53\u306e\u5305\u62ec\u7684\u306a\u8a55\u4fa1\u306b\u306f\u65b0\u305f\u306a\u30e1\u30bd\u30c3\u30c9\u304c\u5fc5\u8981\u3067\u3059\u3002\u305d\u3053\u3067\u79c1\u305f\u3061\u306f\u3001\u30d2\u30c8\u8840\u6f3f\u304a\u3088\u3073\u8840\u6e05\u4e2d\u306eC1\u301cC10 PFAS<\/strong>\u306e\u5b9a\u91cf\u306b\u304a\u3044\u3066\u9ad8\u3044\u6709\u52b9\u6027\u3092\u793a\u3057\u305f\u3001\u6975\u6027\u57fa\u5c0e\u5165\u578b\u9006\u76f8LC\u30ab\u30e9\u30e0\u306e\u30a2\u30d7\u30ed\u30fc\u30c1\u3092\u5fdc\u7528\u3057\u3001\u6c34\u30de\u30c8\u30ea\u30c3\u30af\u30b9\u4e2d\u3067\u3082C1\u301cC14 PFAS<\/strong>\u3092\u540c\u6642\u5206\u6790\u53ef\u80fd\u306a\u65b0\u305f\u306a\u624b\u6cd5\u3092\u958b\u767a\u3057\u307e\u3057\u305f\u3002<\/p>\n\n\n\n

\u65b0\u305f\u306b\u958b\u767a\u3057\u305f\u30e1\u30bd\u30c3\u30c9\u3067\u306f\u3001\u6975\u6027\u5316\u5408\u7269\u306e\u4fdd\u6301\u304c\u53ef\u80fd\u306a\u30ab\u30e9\u30e0\u56fa\u5b9a\u76f8\u3068\u3001\u4e0d\u6d3b\u6027\u30b3\u30fc\u30c6\u30a3\u30f3\u30b0\u304c\u65bd\u3055\u308c\u305f\u30cf\u30fc\u30c9\u30a6\u30a7\u30a2\u3092\u7d44\u307f\u5408\u308f\u305b\u305fUltra IBD Inert\u30ab\u30e9\u30e0<\/a>\u3092\u7528\u3044\u307e\u3057\u305f\u3002\u305d\u306e\u7d50\u679c\u3001C1\u301cC14<\/strong>\u306e\u30d1\u30fc\u30d5\u30eb\u30aa\u30ed\u30ab\u30eb\u30dc\u30f3\u9178\u985e\u304a\u3088\u3073\u30b9\u30eb\u30db\u30f3\u9178\u985e\u3092\u5bfe\u8c61\u3068\u3057\u305f\u3001\u30b7\u30f3\u30d7\u30eb\u3067\u518d\u73fe\u6027\u306e\u9ad8\u3044\u540c\u6642\u5206\u6790\u304c\u53ef\u80fd\u3068\u306a\u308a\u307e\u3057\u305f\u3002Figure 1<\/strong>\u306b\u793a\u3059\u3088\u3046\u306b\u3001TFA\u306e\u3088\u3046\u306a\u9ad8\u6975\u6027\u5316\u5408\u7269\u3092\u3057\u3063\u304b\u308a\u3068\u4fdd\u6301\u3057\u3001\u91d1\u5c5e\u3068\u306e\u4e0d\u8981\u306a\u76f8\u4e92\u4f5c\u7528\u3092\u6392\u9664\u3059\u308b\u3053\u3068\u3067\u3001\u30d4\u30fc\u30af\u5f62\u72b6\u3082\u6539\u5584\u3057\u3066\u3044\u307e\u3059\u3002\u7279\u306b\u3001PFBA\u306a\u3069\u306e\u77ed\u9396PFAS<\/strong>\u3092\u6709\u6a5f\u6eb6\u5a92\u6bd4\u7387\u306e\u9ad8\u3044\u30b5\u30f3\u30d7\u30eb\u6eb6\u6db2\u4e2d\u3067\u5206\u6790\u3059\u308b\u969b\u306b\u3082\u3001\u826f\u597d\u306a\u30d4\u30fc\u30af\u5f62\u72b6\u304c\u5f97\u3089\u308c\u3066\u304a\u308a\u3001\u591a\u69d8\u306aPFAS\u306e\u5305\u62ec\u7684\u306a\u5206\u6790\u3092\u9ad8\u3044\u7cbe\u5ea6\u3067\u5206\u6790\u3059\u308b\u3053\u3068\u304c\u3067\u304d\u307e\u3059\u3002<\/p>\n\n\n

Figure 1<\/strong>:\u00a0\u6c34\u30de\u30c8\u30ea\u30c3\u30af\u30b9\u4e2d\u306e\uff08\u8d85\u77ed\u9396PFAS\u3092\u542b\u3080\uff09PFAS\u5305\u62ec\u7684\u5206\u6790\u3092Ultra IBD Inert\u30ab\u30e9\u30e0\u3067\u884c\u3044\u307e\u3057\u305f\uff08\u30d4\u30fc\u30af\u30ea\u30b9\u30c8\u3068\u5206\u6790\u6761\u4ef6\u3092\u542b\u3080\u5b8c\u5168\u7248\u306fPDF\u3067\u30c0\u30a6\u30f3\u30ed\u30fc\u30c9\u53ef\uff09\u3002\u30d4\u30fc\u30af\u756a\u53f7\u306f\u70ad\u9396\u9577\u3092\u793a\u3057\u3066\u3044\u307e\u3059\u3002<\/div>
\n
\"Incorporating<\/div>

LC_EV0597<\/p>

<\/path><\/g><\/path><\/g><\/svg>Download PDF<\/a><\/div><\/div><\/div>\n<\/div><\/div><\/div>\n\n\n
<\/div>\n\n\n\n

\u77ed\u9396\uff5e\u9577\u9396PFAS\u306e\u8fc5\u901f\u306a\u5206\u6790\u3092\u53ef\u80fd\u306b\u3059\u308bC18\u30ab\u30e9\u30e0<\/h2>\n\n\n\n

\u77ed\u9396PFAS(C4~C6)<\/strong>\u3068\u305d\u308c\u4ee5\u4e0a\u306b\u3064\u3044\u3066\u306f\u3001\u7570\u306a\u308b\u56fa\u5b9a\u76f8\u306e\u30b9\u30ab\u30a6\u30c6\u30a3\u30f3\u30b0\u306b\u3088\u308a\u3001C18\u304c\u6700\u9069\u306a\u9078\u629e\u3067\u3042\u308b\u3053\u3068\u304c\u793a\u3055\u308c\u307e\u3057\u305f\u3002PFAS\u5206\u5b50\u306e\u30a2\u30eb\u30ad\u30eb\u9396\u304c\u9577\u304f\u306a\u308b\u306b\u3064\u308c\u3066\u3001\u30a2\u30eb\u30ad\u30eb\u9396\u3068\u5b98\u80fd\u57fa\u3067\u3042\u308bC18\u3068\u306e\u9593\u306e\u76f8\u4e92\u4f5c\u7528\u304c\u5897\u52a0\u3057\u3001\u4fdd\u6301\u304a\u3088\u3073\u5206\u96e2\u306b\u5bfe\u3057\u3066\u826f\u597d\u306a\u30e1\u30ab\u30cb\u30ba\u30e0\u3092\u3082\u305f\u3089\u3057\u307e\u3059\u3002\u6bd4\u8f03\u7684\u77ed\u304f\u3066\u7d30\u3044\u30ab\u30e9\u30e0\u3092\u4f7f\u7528\u3057\u3066\u6a19\u7684\u5206\u6790\u7a2e\u3092\u8fc5\u901f\u304b\u3064\u52b9\u679c\u7684\u306b\u5206\u96e2\u3067\u304d\u308b\u307b\u3069\u306b\u3001\u4fdd\u6301\u306f\u5f37\u529b\u3067\u3059\u3002Figure 2<\/strong>\u306e\u4f8b\u306f\u300150\u00d72.1mm\u306eRaptor C18\u30ab\u30e9\u30e0<\/a>\u304c\u30018\u5206\u672a\u6e80(\u30c8\u30fc\u30bf\u30eb\u5206\u6790\u6642\u959310\u5206\u9593)\u3067\u3001\u76ee\u7684\u5316\u5408\u7269\u3092\u7c21\u5358\u306b\u6eb6\u51fa\u304a\u3088\u3073\u5206\u96e2\u3057\u3001\u98f2\u6599\u6c34\u8a66\u9a13\u6cd5EPA 537.1\u306e\u57fa\u6e96\u3092\u5168\u3066\u3092\u6e80\u305f\u3057\u3066\u3044\u308b\u3053\u3068\u3092\u793a\u3057\u3066\u3044\u307e\u3059\u3002<\/p>\n\n\n

Figure 2<\/strong>:50 x 2.1 mm Raptor C18 column \u306f\u3001\u512a\u308c\u305fPFAS LC\u30ab\u30e9\u30e0\u306e\u9078\u629e\u80a2\u3067\u3042\u308a\u300110\u5206\u306e\u8fc5\u901f\u306a\u30c8\u30fc\u30bf\u30eb\u30b5\u30a4\u30af\u30eb\u30bf\u30a4\u30e0\u3067EPA537.1\u30e1\u30bd\u30c3\u30c9\u57fa\u6e96\u3092\u5168\u3066\u6e80\u305f\u3057\u307e\u3059\uff08\u30d4\u30fc\u30af\u30ea\u30b9\u30c8\u3068\u5206\u6790\u6761\u4ef6\u3092\u542b\u3080\u5b8c\u5168\u7248\u306fPDF\u3067\u30c0\u30a6\u30f3\u30ed\u30fc\u30c9\u53ef\uff09\u3002<\/div>
\n
\"EPA<\/div>

LC_EV0560<\/p>

<\/path><\/g><\/path><\/g><\/svg>Download PDF<\/a><\/div><\/div><\/div>\n<\/div><\/div><\/div>\n\n\n
<\/div>\n\n\n\n

\u8d85\u77ed\u9396PFAS\u306b\u306f\u9069\u5207\u306a\u30ab\u30e9\u30e0\u30b5\u30a4\u30ba\u306eC18\u3001\u307e\u305f\u306fRaptor Polar X\u3092<\/h2>\n\n\n\n

C8\u306ePFAS\u304c\u7981\u6b62\u3055\u308c\u308b\u3068\u3001\u3088\u308a\u77ed\u3044\u30a2\u30eb\u30ad\u30eb\u9396\u3092\u6709\u3059\u308b\u4ed6\u306e\u5316\u5408\u7269\u304c\u5546\u696d\u7684\u306b\u63a1\u7528\u3055\u308c\u307e\u3057\u305f\u3002\u95a2\u5fc3\u306e\u3042\u308bPFAS\u30ea\u30b9\u30c8\u304c\u5897\u3048\u308b\u306b\u3064\u308c\u3066\u3001\u70ad\u7d20\u6570\u304c4\u3088\u308a\u77ed\u3044\u9396\u3092\u6709\u3059\u308b\u5316\u5408\u7269\u3001\u307e\u305f\u306f\u300c\u8d85\u77ed\u9396\u300d(C2\u304a\u3088\u3073C3)<\/strong>\u304c\u3088\u308a\u6ce8\u76ee\u3092\u96c6\u3081\u3066\u3044\u307e\u3059\u3002\u70ad\u7d20\u9396\u306e\u9577\u3055\u304c\u6e1b\u5c11\u3059\u308b\u306b\u3064\u308c\u3066\u3001\u6975\u6027\u672b\u7aef\u306e\u5f71\u97ff\u304c\u5927\u304d\u304f\u306a\u308a\u3001\u6700\u7d42\u7684\u306b\u306f\u3001\u4e3b\u306b\u758e\u6c34\u6027\u76f8\u4e92\u4f5c\u7528\u306b\u57fa\u3065\u304f\u4fdd\u6301\u30e1\u30ab\u30cb\u30ba\u30e0\u3092\u6709\u3059\u308bC18\u30ab\u30e9\u30e0\u3067\u306e\u4fdd\u6301\u306f\u6e1b\u5c11\u3057\u307e\u3059\u3002<\/p>\n\n\n\n

\u30d1\u30fc\u30d5\u30eb\u30aa\u30ed\u30d7\u30ed\u30d1\u30f3\u9178(PFPrA)\u304a\u3088\u3073\u30d1\u30fc\u30d5\u30eb\u30aa\u30ed\u30d7\u30ed\u30d1\u30f3\u30b9\u30eb\u30db\u30f3\u9178(PFPrS)\u306e\u3088\u3046\u306aC3\u306ePFAS\u5316\u5408\u7269<\/strong>\u306b\u304a\u3044\u3066\u306f\u3001\u9069\u5207\u306a\u30ab\u30e9\u30e0\u30b5\u30a4\u30ba\u304c\u9078\u629e\u3055\u308c\u308c\u3070\u3001C18\u304c\u4f9d\u7136\u3068\u3057\u3066\u6a5f\u80fd\u3057\u307e\u3059\u3002\u4f8b\u3048\u3070\u3001Figure 3<\/strong>\u3067\u306f\u3001100\u00d73 mm\u306eRaptor C18<\/a>\u304c\u512a\u308c\u305f\u6027\u80fd\u3092\u793a\u3057\u3066\u304a\u308a\u300111\u5206\u9593\u306e\u8fc5\u901f\u306a\u5206\u6790\u3067C3\u306ePFAS<\/strong>\u3092\u7c21\u5358\u306b\u7d44\u307f\u8fbc\u3081\u3066\u3044\u307e\u3059\u3002<\/p>\n\n\n

Figure 3<\/strong>: Raptor C18\u56fa\u5b9a\u76f8\u306f\u77ed\u9396PFAS\u3082\u52b9\u679c\u7684\u306b\u5206\u96e2\u3057\u307e\u3059\u304c\u3001\u9069\u5207\u306a\u4fdd\u6301\u3092\u78ba\u4fdd\u3059\u308b\u306b\u306f\u30ab\u30e9\u30e0\u30b5\u30a4\u30ba\u3092\u5927\u304d\u304f\u3059\u308b\u5fc5\u8981\u304c\u3042\u308a\u307e\u3059\uff08\u30d4\u30fc\u30af\u30ea\u30b9\u30c8\u3068\u5206\u6790\u6761\u4ef6\u3092\u542b\u3080\u5b8c\u5168\u7248\u306fPDF\u3067\u30c0\u30a6\u30f3\u30ed\u30fc\u30c9\u53ef\uff09\u3002<\/div>
\n
\"Ultra-short<\/div>

LC_EV0555<\/p>

<\/path><\/g><\/path><\/g><\/svg>Download PDF<\/a><\/div><\/div><\/div>\n<\/div><\/div><\/div>\n\n\n
<\/div>\n\n\n\n

C2\u306ePFAS<\/strong>(\u4f8b\u3048\u3070\u3001\u30c8\u30ea\u30d5\u30eb\u30aa\u30ed\u9162\u9178)\u304c\u6700\u7d42\u7684\u306b\u76e3\u8996\u5bfe\u8c61\u5316\u5408\u7269\u306e\u30ea\u30b9\u30c8\u306b\u542b\u307e\u308c\u308b\u5834\u5408\u306f\u3001PFAS\u5206\u5b50\u306e\u6975\u6027\u90e8\u5206\u3092\u30bf\u30fc\u30b2\u30c3\u30c8\u3068\u3059\u308b\u5225\u306e\u56fa\u5b9a\u76f8\u304c\u5fc5\u8981\u3067\u3059\u3002C18\u30ab\u30e9\u30e0\u306e\u4e3b\u305f\u308b\u758e\u6c34\u6027\u76f8\u4e92\u4f5c\u7528\u304b\u3089\u3001\u30a4\u30aa\u30f3\u4ea4\u63db\u304a\u3088\u3073HILIC\u5206\u96e2\u30e2\u30fc\u30c9\u306e\u4e21\u65b9\u304c\u53ef\u80fd\u306a\u56fa\u5b9a\u76f8\u3092\u6709\u3059\u308bRaptor Polar X\u30ab\u30e9\u30e0\u306b\u5207\u308a\u66ff\u3048\u308b\u3053\u3068\u3067\u3001\u8d85\u77ed\u9396PFAS<\/strong>\u306e\u4fdd\u6301\u304c\u53ef\u80fd\u306b\u306a\u308a\u307e\u3059\u3002 Raptor Polar X\u30ab\u30e9\u30e0<\/a>\u306f\u3001Figure 4<\/strong>\u306b\u793a\u3059\u3088\u3046\u306b\u3001\u8d85\u77ed\u9396PFAS<\/strong>\u306b\u52a0\u3048\u3066\u3001\u540c\u3058\u5206\u6790\u3067\u77ed\u9396\u3001\u9577\u9396\u3001\u304a\u3088\u3073\u4ee3\u66ffPFAS\u5316\u5408\u7269<\/strong>\u3092\u4fdd\u6301\u304a\u3088\u3073\u5206\u96e2\u3059\u308b\u3053\u3068\u3082\u3067\u304d\u3001\u6700\u3082\u5305\u62ec\u7684\u306a\u4e00\u6589\u5206\u6790\u306ePFAS\u30e1\u30bd\u30c3\u30c9\u3092\u63d0\u4f9b\u3057\u307e\u3059\u3002<\/p>\n\n\n

Figure 4:<\/strong>\u00a0Raptor Polar X\u30ab\u30e9\u30e0\u306f\u3001\u8907\u6570\u306e\u4fdd\u6301\u30e2\u30fc\u30c9\u3092\u5229\u7528\u3057\u3066\u304a\u308a\u3001\u5358\u4e00\u30e1\u30bd\u30c3\u30c9\u3067\u8d85\u77ed\u9396\u3001\u9577\u9396\u3001\u304a\u3088\u3073\u4ee3\u66ffPFAS\u3092\u5206\u6790\u3059\u308b\u306e\u306b\u6700\u9069\u3067\u3059\uff08\u30d4\u30fc\u30af\u30ea\u30b9\u30c8\u3068\u5206\u6790\u6761\u4ef6\u3092\u542b\u3080\u5b8c\u5168\u7248\u306fPDF\u3067\u30c0\u30a6\u30f3\u30ed\u30fc\u30c9\u53ef\uff09\u3002<\/div>
\n
\"Ultrashort-<\/div>

LC_EV0569<\/p>

<\/path><\/g><\/path><\/g><\/svg>Download PDF<\/a><\/div><\/div><\/div>\n<\/div><\/div><\/div>\n\n\n
<\/div>\n\n\n\n

\u30ab\u30e9\u30e0\u7c92\u5b50\u30b5\u30a4\u30ba\u304a\u3088\u3073\u7c92\u5b50\u30bf\u30a4\u30d7\u306e\u9078\u629e<\/h2>\n\n\n\n

\u56fa\u5b9a\u76f8\u3068\u30ab\u30e9\u30e0\u30b5\u30a4\u30ba\u306b\u52a0\u3048\u3066\u3001\u7c92\u5b50\u5f84\u304a\u3088\u3073\u7a2e\u985e\u306b\u3064\u3044\u3066\u306e\u9078\u629e\u3082\u5fc5\u8981\u3067\u3059\u3002\u6700\u7d42\u7684\u306b\u306f\u3001Raptor\u30ab\u30e9\u30e0\u306b\u4f7f\u308f\u308c\u308b\u3066\u3044\u308b\u3088\u3046\u306a2.7\u03bcm\u306e\u8868\u9762\u591a\u5b54\u6027\u7c92\u5b50(SPP)<\/strong>\u304c\u6700\u3082\u6c4e\u7528\u6027\u306e\u9ad8\u3044\u9078\u629e\u3067\u3059\u3002\u3053\u306e\u30bf\u30a4\u30d7\u306e\u7c92\u5b50\u3067\u4f5c\u88fd\u3055\u308c\u305fPFAS LC\u30ab\u30e9\u30e0\u306f\u3001\u8d85\u9ad8\u5727\u306b\u306a\u308b\u3053\u3068\u306a\u304f\u30b5\u30d62\u03bcm\u306e\u5168\u591a\u5b54\u6027\u7c92\u5b50(FPP)<\/strong>\u306b\u5339\u6575\u3059\u308b\u52b9\u7387\u7684\u306a\u30af\u30ed\u30de\u30c8\u30b0\u30e9\u30d5\u30a3\u30fc\u3092\u751f\u6210\u3057\u307e\u3059\u3002\u3053\u308c\u306b\u3088\u308a\u3001\u30e9\u30dc\u306fUHPLC\u307e\u305f\u306fHPLC\u6a5f\u5668<\/strong>\u306e\u3044\u305a\u308c\u3067\u3082\u8fc5\u901f\u3067\u52b9\u7387\u7684\u306a\u5206\u6790\u3092\u304a\u3053\u306a\u3046\u3053\u3068\u304c\u3067\u304d\u307e\u3059\u3002<\/p>\n\n\n\n

\u305f\u3060\u3057\u3001\u7c92\u5b50\u5f84\u3068\u7a2e\u985e\u306e\u9078\u629e\u306f\u3001\u6a5f\u5668\u306e\u8a2d\u5b9a\u306b\u5fdc\u3058\u3066\u305d\u306e\u52b9\u679c\u304c\u5927\u304d\u304f\u306a\u3063\u305f\u308a\u5c0f\u3055\u304f\u306a\u3063\u305f\u308a\u3057\u307e\u3059\u3002 \u4f8b\u3048\u3070\u3001\u5f93\u6765\u306eHPLC\u6a5f\u5668<\/strong>\u3092\u4f7f\u7528\u3057\u30015\u03bcm\u306eFPP\u30ab\u30e9\u30e0<\/strong>\u3092\u65e5\u9803\u4f7f\u7528\u3057\u3066\u3044\u308b\u5834\u5408\u306f\u3001\u7c92\u5f84\u306b\u95a2\u4fc2\u306a\u304f\u3001SPP\u30ab\u30e9\u30e0\u304c\u3082\u305f\u3089\u3059\u6539\u5584\u306b\u9a5a\u304b\u308c\u308b\u304b\u3082\u3057\u308c\u307e\u305b\u3093\u3002SPP\u30ab\u30e9\u30e0<\/strong>\u3092\u4f7f\u7528\u3059\u308b\u3068\u3001\u307b\u3068\u3093\u3069\u306eHPLC\u6a5f\u5668<\/strong>\u306e\u5727\u529b\u7bc4\u56f2\u3067\u3001\u30af\u30ed\u30de\u30c8\u30b0\u30e9\u30d5\u30a3\u30fc\u52b9\u7387\u306e\u5411\u4e0a\u3068\u30d4\u30fc\u30af\u5f62\u72b6\u306e\u6539\u5584\u3092\u7c21\u5358\u306b\u78ba\u8a8d\u3067\u304d\u307e\u3059\u3002 \u540c\u3058\u6a5f\u5668\u306b\u3088\u308b\u9ad8\u901f\u5206\u6790\u306f\u3001UHPLC\u6a5f\u5668\u306b\u8a2d\u5099\u6295\u8cc7\u3059\u308b\u3053\u3068\u306a\u304f\u30b5\u30f3\u30d7\u30eb\u30b9\u30eb\u30fc\u30d7\u30c3\u30c8\u3092\u5411\u4e0a\u3055\u305b\u308b\u3053\u3068\u306b\u95a2\u5fc3\u306e\u3042\u308b\u591a\u304f\u306e\u30e9\u30dc\u306b\u3068\u3063\u3066\u3001\u512a\u308c\u305f\u7d44\u5408\u305b\u3067\u3059\u3002<\/p>\n\n\n\n

\u3059\u3067\u306bUHPLC\u6a5f\u5668<\/strong>\u3092\u4f7f\u7528\u3057\u3066\u3044\u308b\u30e9\u30dc\u3067\u306f\u3001\u7279\u306bSPP\u30ab\u30e9\u30e0\u306b\u304a\u3051\u308b\u7c92\u5b50\u5f84\u306e\u9078\u629e\u304c\u52b9\u7387\u3068\u5206\u6790\u6642\u9593\u306b\u5dee\u3092\u3082\u305f\u3089\u3059\u3053\u3068\u306f\u3042\u307e\u308a\u306a\u3044\u3067\u3057\u3087\u3046\u3002Figure 5<\/strong>\u306f\u3001UHPLC\u30b7\u30b9\u30c6\u30e0\u3092\u4f7f\u7528\u3057\u3066PFAS\u5206\u6790\u3092\u304a\u3053\u306a\u3063\u305f\u5834\u5408\u306e\u30013\u7a2e\u985e\u306eRaptor SPP\u30ab\u30e9\u30e0\u306b\u3088\u308b\u7c92\u5b50\u5f84\u306e\u5f71\u97ff\u3092\u793a\u3057\u305f\u3082\u306e\u3067\u3059\u3002\u4e00\u822c\u7684\u306a\u30af\u30ed\u30de\u30c8\u30b0\u30e9\u30d5\u30a3\u30fc\u539f\u7406\u306b\u3042\u308b\u3088\u3046\u306b\u3001\u30d4\u30fc\u30af\u306f1.8 \u03bcm\u7c92\u5b50\u30ab\u30e9\u30e0<\/a><\/strong>\u3067\u6700\u3082\u72ed\u304f\u306a\u3063\u3066\u3044\u307e\u3059\u304c\u30015 \u03bcm\u30ab\u30e9\u30e0<\/a><\/strong>\u30681.8 \u03bcm\u30ab\u30e9\u30e0<\/strong>\u306b\u304a\u3051\u308b\u52b9\u7387\u306e\u5dee\u306f\u5927\u304d\u304f\u306f\u3042\u308a\u307e\u305b\u3093\u3067\u3057\u305f\u3002 \u3057\u304b\u3057\u3001\u3053\u306e\u3088\u3046\u306b\u975e\u5e38\u306b\u826f\u304f\u4f3c\u305f\u7d50\u679c\u3092\u9054\u6210\u3059\u308b\u4e0a\u3067\u751f\u6210\u3055\u308c\u308b\u80cc\u5727\u306e\u5dee\u7570\u306f\u5927\u304d\u304f\u30015\u304a\u3088\u30732.7\u03bcm\u7c92\u5b50\u306e\u30ab\u30e9\u30e0<\/a><\/strong>\u3067\u306f\u3001\u5727\u529b\u306f\u5f93\u6765\u306eHPLC\u6a5f\u5668<\/strong>\u306e\u7bc4\u56f2\u5185\u3067\u3059\u3002 \u3053\u308c\u3089\u306e\u7c92\u5b50\u3092\u5145\u586b\u3057\u305fPFAS LC\u30ab\u30e9\u30e0\u3092\u4f7f\u7528\u3059\u308b\u3068\u3001\u8d85\u9ad8\u5727\u306b\u306a\u3089\u305a\u306bUHPLC\u6027\u80fd\u3092\u5f97\u308b\u3053\u3068\u304c\u3067\u304d\u307e\u3059\u3002<\/p>\n\n\n

Figure 5<\/strong>: SPP\u30ab\u30e9\u30e0\u3067\u306f\u3001\u7570\u306a\u308b\u7c92\u5b50\u30b5\u30a4\u30ba\u3067\u3082\u540c\u69d8\u306e\u30af\u30ed\u30de\u30c8\u30b0\u30e9\u30d5\u30a3\u30fc\u6027\u80fd\u3092\u5f97\u3089\u308c\u307e\u3059\u304c\u30012.7\u307e\u305f\u306f5 \u03bcm\u306e\u7c92\u5b50\u30ab\u30e9\u30e0\u3092\u9078\u629e\u3059\u308b\u3068\u3001\u80cc\u5727\u304c\u5f93\u6765\u306eHPLC\u30b7\u30b9\u30c6\u30e0\u306e\u7bc4\u56f2\u5185\u306b\u306a\u308a\u307e\u3059(\u3059\u3079\u3066\u306e\u30ab\u30e9\u30e0\u306f50 mm x 2.1 mm\u3067\u3059)\u3002<\/div>
\n\n

1.8 \u00b5m Raptor C18<\/strong>
6500\u20138000 psi<\/p>\n\n\n

\"Perfluorinated<\/div>

LC_EV0540<\/p>

<\/path><\/g><\/path><\/g><\/svg>Download PDF<\/a><\/div><\/div><\/div>\n\n\n

2.7 \u00b5m Raptor C18<\/strong>
4000\u20135500 psi<\/p>\n\n\n

\"Perfluorinated<\/div>

LC_EV0551<\/p>

<\/path><\/g><\/path><\/g><\/svg>Download PDF<\/a><\/div><\/div><\/div>\n\n\n

5 \u00b5m Raptor C18<\/strong>
2000\u20133500 psi<\/p>\n\n\n

\"Perfluorinated<\/div>

LC_EV0541<\/p>

<\/path><\/g><\/path><\/g><\/svg>Download PDF<\/a><\/div><\/div><\/div>\n<\/div><\/div><\/div>\n\n\n
<\/div>\n\n\n\n

\u30b7\u30b9\u30c6\u30e0\u5727\u529b\u3092\u3067\u304d\u308b\u3060\u3051\u4f4e\u304f\u4fdd\u3061\u306a\u304c\u3089\u3001\u6700\u3082\u52b9\u7387\u3092\u826f\u304f\u3059\u308b(\u3053\u308c\u306f\u591a\u304f\u306e\u5834\u5408\u5206\u6790\u6642\u9593\u306e\u77ed\u7e2e\u306b\u3064\u306a\u304c\u308a\u307e\u3059)\u306b\u306f\u3001SPP\u7c92\u5b50<\/strong>\u306ePFAS LC\u30ab\u30e9\u30e0\u304c\u660e\u3089\u304b\u306b\u6709\u5229\u3067\u3059\u3002 \u3057\u304b\u3057\u3001\u591a\u304f\u306e\u30e9\u30dc\u304cFPP\u30ab\u30e9\u30e0<\/strong>\u3092\u9577\u5e74\u4f7f\u7528\u3057\u3066\u304d\u3066\u304a\u308a\u3001\u305d\u306e\u4f7f\u7528\u3092\u7d99\u7d9a\u3057\u3066\u3044\u304f\u3053\u3068\u304c\u597d\u307e\u308c\u308b\u5834\u5408\u3082\u3042\u308a\u307e\u3059\u3002FPP\u30ab\u30e9\u30e0\u3092\u4f7f\u7528\u3057\u3066\u3082\u3001PFAS\u5206\u6790\u306f\u554f\u984c\u306a\u304f\u5b9f\u65bd\u3067\u304d\u307e\u3059\u3002Force C18\u30ab\u30e9\u30e0\u306e\u3088\u3046\u306aFPP\u30ab\u30e9\u30e0<\/a><\/strong>\u3067\u306f\u3001\u8868\u9762\u7a4d\u304c\u3088\u308a\u5927\u304d\u304f\u3001\u70ad\u7d20\u542b\u6709\u91cf\u3082\u9ad8\u3044\u3053\u3068\u306b\u3088\u308a\u3001\u985e\u4f3c\u306e\u7c92\u5f84\u306eSPP\u30ab\u30e9\u30e0(Raptor C18)<\/a><\/strong>\u3068\u6bd4\u8f03\u3057\u3066\u3001\u30af\u30ed\u30de\u30c8\u30b0\u30e9\u30d5\u30a3\u30fc\u4fdd\u6301\u306f\u5f37\u304f\u306a\u308a\u307e\u3059(Figure 6<\/strong>)\u3002<\/p>\n\n\n

Figure 6<\/strong>: FPP\u30ab\u30e9\u30e0\u304c\u671b\u307e\u3057\u3044\u5834\u5408\u3001Force C18\u30ab\u30e9\u30e0\u306fPFAS\u5206\u6790\u306b\u52b9\u679c\u7684\u306a\u5206\u96e2\u3092\u63d0\u4f9b\u3057\u307e\u3059(\u3059\u3079\u3066\u306e\u30ab\u30e9\u30e0\u306f50 mm x 2.1 mm\u3067\u3059)\u3002<\/div>
\n\n

1.8 \u00b5m Raptor C18<\/strong>
6500\u20138000 psi<\/p>\n\n\n

\"Perfluorinated<\/div>

LC_EV0540<\/p>

<\/path><\/g><\/path><\/g><\/svg>Download PDF<\/a><\/div><\/div><\/div>\n\n\n

1.8 \u00b5m Force C18<\/strong>
7550\u20139250 psi<\/p>\n\n\n

\"Perfluorinated<\/div>

LC_EV0552<\/p>

<\/path><\/g><\/path><\/g><\/svg>Download PDF<\/a><\/div><\/div><\/div>\n<\/div><\/div><\/div>\n\n\n
<\/div>\n\n\n\n

\u307e\u3068\u3081\uff1aPFAS\u5206\u6790\u30ab\u30e9\u30e0\u9078\u629e\u306e\u6307\u91dd<\/h2>\n\n\n\n

PFAS LC\u30ab\u30e9\u30e0\u3092\u9078\u629e\u3059\u308b\u5834\u5408\u30012.7\u03bcm\u306eRaptor SPP\u30ab\u30e9\u30e0<\/strong>\u306f\u3001\u512a\u308c\u305f\u5206\u96e2\u5ea6\u3001\u77ed\u3044\u5206\u6790\u6642\u9593\u3001\u304a\u3088\u3073UHPLC\u3068HPLC\u6a5f\u5668\u306e\u4e21\u65b9\u3068\u306e\u9069\u5408\u6027\u3092\u5b9f\u73fe\u3057\u307e\u3059\u3002\u56fa\u5b9a\u76f8\u306e\u9078\u629e\u306f\u3001\u30e2\u30cb\u30bf\u30fc\u5bfe\u8c61\u306ePFAS\u306e\u7bc4\u56f2\u306b\u4f9d\u5b58\u3057\u3066\u304a\u308a\u3001Raptor C18\u30ab\u30e9\u30e0<\/a><\/strong>\u306f\u3001C3\u307e\u3067\u306ePFAS\u306b\u306f\u3001\u512a\u308c\u305f\u9078\u629e\u80a2\u3067\u3059\u3002\u3057\u304b\u3057\u3001\u8d85\u77ed\u9396(C2~C3)PFAS\u4ee5\u4e0a\u306e\u5168\u7bc4\u56f2\u3001\u306a\u3089\u3073\u306b\u4ee3\u66ffPFAS\u3092\u542b\u3080\u6700\u3082\u5305\u62ec\u7684\u306a\u4e00\u6589\u5206\u6790\u306b\u306f\u3001Raptor Polar X\u30ab\u30e9\u30e0<\/a><\/strong>\u304c\u6700\u9069\u3067\u3059\u3002\u8d85\u77ed\u9396\uff5e\u9577\u9396PFAS\u3092\u5206\u6790\u3059\u308b\u5834\u5408\u306b\u304a\u3044\u3066\u306f\u3001Ultra IBD Inert<\/strong>\u30ab\u30e9\u30e0<\/a>\u304c\u6709\u52b9\u306a\u9078\u629e\u80a2\u3068\u306a\u308a\u307e\u3059\u3002<\/strong><\/p>\n\n\n\n

RaptorC18\u30ab\u30e9\u30e0\u304a\u3088\u3073Ultra IBD Inert<\/strong>\u30ab\u30e9\u30e0\u3092\u7528\u3044\u305f<\/strong>\u5fae\u91cf\u5206\u6790\u3067\u306f\u3001PFAS\u30c7\u30a3\u30ec\u30a4\u30ab\u30e9\u30e0<\/a><\/strong>\u3092\u53d6\u4ed8\u3051\u308b\u3053\u3068\u306b\u3088\u3063\u3066\u3001\u507d\u967d\u6027\u307e\u305f\u306f\u5fdc\u7b54\u5024\u306e\u5897\u5927\u3092\u8efd\u6e1b\u3067\u304d\u308b\u3053\u3068\u306b\u3054\u7559\u610f\u304f\u3060\u3055\u3044\u3002PFAS\u30c7\u30a3\u30ec\u30a4\u30ab\u30e9\u30e0\u3092\u4f7f\u7528\u3059\u308b\u3053\u3068\u3067\u3001\u30b5\u30f3\u30d7\u30eb\u4e2d\u306ePFAS\u3068\u5171\u6eb6\u51fa\u3057\u3066\u3057\u307e\u3046\u3001\u30b7\u30b9\u30c6\u30e0\u7531\u6765\u306e\u30d0\u30c3\u30af\u30b0\u30e9\u30a6\u30f3\u30c9PFAS\u6c5a\u67d3\u7269\u8cea\u3092\u6392\u9664\u3057\u307e\u3059\u3002<\/p>\n\n\n\n

\u5f15\u7528\u6587\u732e<\/h2>\n\n\n\n

[1] S.-H. Liang, J.A. Steimling, Integration of ultrashort-chain compounds into the biomonitoring of per- and polyfluorinated substances in human plasma and serum, J. Chromatogr. Open 5 (2024) 100132, https:\/\/doi.org\/10.1016\/j.jcoa.2024.100132<\/a><\/p>\n\n\n\n

<\/div>\n\n\n
\n

Products Mentioned<\/h3>\n
\n
\n
\n
\n Catalog No. 9304A52 <\/a> <\/div>\n
\n
Raptor C18, 2.7 \u00b5m, 50 x 2.1 mm HPLC\u30ab\u30e9\u30e0<\/div>\n <\/div>\n
\n \u88fd\u54c1\u60c5\u5831\u3092\u898b\u308b<\/a>\n <\/div>\n <\/div>\n
\n
\n Catalog No. 9304A1E <\/a> <\/div>\n
\n
Raptor C18, 2.7 \u00b5m, 100 x 3.0 mm HPLC\u30ab\u30e9\u30e0<\/div>\n <\/div>\n
\n \u88fd\u54c1\u60c5\u5831\u3092\u898b\u308b<\/a>\n <\/div>\n <\/div>\n
\n
\n Catalog No. 9311A52 <\/a> <\/div>\n
\n
Raptor Polar X, 2.7 \u00b5m, 50 x 2.1 mm LC\u30ab\u30e9\u30e0<\/div>\n <\/div>\n
\n \u88fd\u54c1\u60c5\u5831\u3092\u898b\u308b<\/a>\n <\/div>\n <\/div>\n
\n
\n Catalog No. 9634252 <\/a> <\/div>\n
\n
Force C18, 1.8 \u00b5m, 50 x 2.1 mm LC\u30ab\u30e9\u30e0<\/div>\n <\/div>\n
\n \u88fd\u54c1\u60c5\u5831\u3092\u898b\u308b<\/a>\n <\/div>\n <\/div>\n
\n
\n Catalog No. 9304552 <\/a> <\/div>\n
\n
Raptor C18, 5 \u00b5m, 50 x 2.1 mm HPLC\u30ab\u30e9\u30e0<\/div>\n <\/div>\n
\n \u88fd\u54c1\u60c5\u5831\u3092\u898b\u308b<\/a>\n <\/div>\n <\/div>\n
\n
\n Catalog No. 9304252 <\/a> <\/div>\n
\n
Raptor C18, 1.8 \u00b5m, 50 x 2.1 mm HPLC\u30ab\u30e9\u30e0<\/div>\n <\/div>\n
\n \u88fd\u54c1\u60c5\u5831\u3092\u898b\u308b<\/a>\n <\/div>\n <\/div>\n <\/div>\n <\/div>\n \n\n\n
<\/div>\n","protected":false},"excerpt":{"rendered":"

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