{"id":43628,"date":"2021-06-25T14:30:00","date_gmt":"2021-06-25T14:30:00","guid":{"rendered":"https:\/\/discover.restek.com\/uncategorized\/japanese-revive-in-line-sample-preparation-ilsp-a-faster-approach-for-multiresidue-pesticides-in-food\/"},"modified":"2025-11-25T22:24:59","modified_gmt":"2025-11-25T22:24:59","slug":"japanese-revive-in-line-sample-preparation-ilsp-a-faster-approach-for-multiresidue-pesticides-in-food","status":"publish","type":"post","link":"https:\/\/discover.restek.com\/ja\/articles-ja\/fsss3549-ja\/japanese-revive-in-line-sample-preparation-ilsp-a-faster-approach-for-multiresidue-pesticides-in-food","title":{"rendered":"Revive\u30a4\u30f3\u30e9\u30a4\u30f3\u30b5\u30f3\u30d7\u30eb\u524d\u51e6\u7406(ILSP): \u98df\u54c1\u4e2d\u306e\u591a\u6210\u5206\u6b8b\u7559\u8fb2\u85ac\u5206\u6790\u306e\u8fc5\u901f\u306a\u30a2\u30d7\u30ed\u30fc\u30c1"},"content":{"rendered":"\n<ul class=\"wp-block-list\">\n<li>\u81ea\u52d5\u5316\u3055\u308c\u305f\u30b5\u30f3\u30d7\u30eb\u62bd\u51fa\u7269\u306e\u30a4\u30f3\u30e9\u30a4\u30f3\u30af\u30ea\u30fc\u30f3\u30a2\u30c3\u30d7\u306f\u3001\u524d\u51e6\u7406\u306b\u304b\u304b\u308b\u6642\u9593\u3092\u5927\u5e45\u306b\u77ed\u7e2e\u3057\u307e\u3059\u3002<\/li>\n\n\n\n<li>\u5206\u6790\u3068ILSP\u30ab\u30fc\u30c8\u30ea\u30c3\u30b8\u6d17\u6d44\u3092\u540c\u6642\u306b\u304a\u3053\u306a\u3046\u3053\u3068\u3067\u3001\u30b5\u30f3\u30d7\u30eb\u9593\u306e\u30c0\u30a6\u30f3\u30bf\u30a4\u30e0\u3092\u306a\u304f\u3057\u307e\u3059\u3002<\/li>\n\n\n\n<li>\u98df\u54c1\u306e\u591a\u6210\u5206\u6b8b\u7559\u8fb2\u85ac\u5206\u6790\u306b\u304a\u3051\u308b\u3001QuEChERS\u3084SPE\u3068\u3044\u3063\u305f\u524d\u51e6\u7406\u306e\u8fc5\u901f\u304b\u3064\u30b7\u30f3\u30d7\u30eb\u306a\u4ee3\u66ff\u6cd5\u3067\u3059\u3002<\/li>\n<\/ul>\n\n\n\n<ul class=\"wp-block-list\">\n<li><\/li>\n<\/ul>\n\n\n\n<p>\u30a4\u30f3\u30e9\u30a4\u30f3\u30b5\u30f3\u30d7\u30eb\u524d\u51e6\u7406(ILSP)\u306f\u3001\u6027\u80fd\u3092\u72a0\u7272\u306b\u3059\u308b\u3053\u3068\u306a\u304f\u3001LC\u2010MS\/MS\u5206\u6790\u3067\u306e\u30b5\u30f3\u30d7\u30eb\u3042\u305f\u308a\u306e\u6642\u9593\u3068\u8cbb\u7528\u306e\u524a\u6e1b\u3092\u6c42\u3081\u3066\u3044\u308b\u98df\u54c1\u5b89\u5168\u30e9\u30dc\u306b\u3068\u3063\u3066\u7406\u60f3\u7684\u306a\u30b5\u30f3\u30d7\u30eb\u524d\u51e6\u7406\u6280\u8853\u3067\u3059\u3002Revive ILSP\u8fb2\u85ac\u30ab\u30fc\u30c8\u30ea\u30c3\u30b8\u306f\u3001\u5f93\u6765\u306eSPE\u304a\u3088\u3073QuEChERS\u30e1\u30bd\u30c3\u30c9\u3068\u540c\u69d8\u306b\u3001\u5e72\u6e09\u3059\u308b\u53ef\u80fd\u6027\u306e\u3042\u308b\u30de\u30c8\u30ea\u30c3\u30af\u30b9\u6210\u5206\u304b\u3089\u5206\u6790\u7a2e\u3092\u5206\u96e2\u3057\u307e\u3059\u3002\u3055\u3089\u306b\u3053\u306e\u624b\u6cd5\u306f\u3001\u6642\u9593\u306e\u304b\u304b\u308b\u624b\u52d5\u624b\u9806\u3092\u3001\u5206\u6790\u30b5\u30f3\u30d7\u30eb\u6d41\u8def\u306b\u6cbf\u3063\u3066\u30b7\u30b9\u30c6\u30e0\u4e0a\u3067\u304a\u3053\u306a\u308f\u308c\u308b\u81ea\u52d5\u30af\u30ea\u30fc\u30f3\u30a2\u30c3\u30d7\u30d7\u30ed\u30bb\u30b9\u306b\u7f6e\u304d\u63db\u3048\u307e\u3059\u3002Revive ILSP\u8fb2\u85ac\u30ab\u30fc\u30c8\u30ea\u30c3\u30b8\u306f\u3001\u52b9\u679c\u7684\u306a\u4fdd\u6301\u6a5f\u69cb(\u4f8b\u3048\u3070\u3001\u9006\u76f8\u76f8\u4e92\u4f5c\u7528)\u3068\u52b9\u7387\u7684\u306a\u7c92\u5b50\u8a2d\u8a08\u3092\u99c6\u4f7f\u3057\u3066\u3044\u307e\u3059\u3002\u3053\u306e\u305f\u3081\u3001\u30b5\u30f3\u30d7\u30eb\u5206\u6790\u3068\u540c\u6642\u306b\u30b7\u30b9\u30c6\u30e0\u4e0a\u3067\u304a\u3053\u306a\u3046\u3053\u3068\u304c\u3067\u304d\u3001\u8907\u96d1\u306a\u30b5\u30f3\u30d7\u30eb\u306b\u5bfe\u3057\u3066\u5f37\u529b\u3067\u81ea\u52d5\u5316\u3055\u308c\u305f\u30af\u30ed\u30de\u30c8\u30b0\u30e9\u30d5\u30a3\u30fc\u30af\u30ea\u30fc\u30f3\u30a2\u30c3\u30d7\u3092\u3082\u305f\u3089\u3057\u307e\u3059\u3002<\/p>\n\n\n\n<p>\u30a4\u30f3\u30e9\u30a4\u30f3\u30b5\u30f3\u30d7\u30eb\u524d\u51e6\u7406\u306e\u5229\u70b9\u306e\u4f8b\u3068\u3057\u3066\u3001\u56f31\u306f\u30db\u30a6\u30ec\u30f3\u30bd\u30a6\u4e2d\u306e\u6b8b\u7559\u8fb2\u85ac\u5206\u6790\u306b\u304a\u3051\u308bRevive ILSP\u3068\u4e00\u822c\u7684\u306aQuEChERS\u306e\u30ef\u30fc\u30af\u30d5\u30ed\u30fc\u3092\u6bd4\u8f03\u3057\u3066\u3044\u307e\u3059\u3002ISLP\u30a2\u30d7\u30ed\u30fc\u30c1\u306b\u3088\u308a\u30b5\u30f3\u30d7\u30eb\u306e\u79fb\u3057\u66ff\u3048\u304c\u5c11\u306a\u304f\u3066\u6e08\u307f\u30011.5\u6642\u9593\u306e\u6642\u9593\u77ed\u7e2e\u3092\u5b9f\u73fe\u3057\u3001\u30b5\u30f3\u30d7\u30eb\u524d\u51e6\u7406\u306e\u751f\u7523\u6027\u304c\u5927\u5e45\u306b\u5411\u4e0a\u3057\u307e\u3057\u305f\u3002ILSP\u306f\u307e\u305f\u3001\u624b\u52d5\u306e\u624b\u9806\u3067\u8d77\u3053\u308a\u3046\u308b\u30a8\u30e9\u30fc\u306e\u30ea\u30b9\u30af\u3092\u6700\u5c0f\u9650\u306b\u3057\u3001QuEChERS\u3068\u6bd4\u8f03\u3057\u3066\u540c\u7b49\u307e\u305f\u306f\u512a\u308c\u305f\u5206\u6790\u7d50\u679c\u3092\u63d0\u4f9b\u3057\u307e\u3059\u3002\u3053\u306e\u6bd4\u8f03\u306e\u7db2\u7f85\u7684\u306a\u7814\u7a76\u306f\u3001Lupo\u3089\u306b\u3088\u3063\u3066\u767a\u8868\u3055\u308c\u3066\u3044\u307e\u3059[1]\u3002<\/p>\n\n\n<div class=\"wp-block-custom-chromatogram-article-top\"><div class=\"chromatogram-article-placeholder\"><div class=\"figure-heading\"><strong>\u56f3 1:<\/strong>\u00a0Revive\u30a4\u30f3\u30e9\u30a4\u30f3\u30b5\u30f3\u30d7\u30eb\u524d\u51e6\u7406\u306f\u3001\u30db\u30a6\u30ec\u30f3\u30bd\u30a6\u30b5\u30f3\u30d7\u30eb14\u500b\u3092\u3001\u5f93\u6765\u306eQuEChERS\u30ef\u30fc\u30af\u30d5\u30ed\u30fc\u3088\u308a\u30821.5\u6642\u9593\u901f\u304f\u51e6\u7406\u3067\u304d\u307e\u3059\u3002\u00a0<\/div><div class='chromatogram-article-inner-full'><div class=\"chromatogram-article-inner\">\n\n<figure class=\"wp-block-image size-large\"><img loading=\"lazy\" decoding=\"async\" width=\"790\" height=\"1024\" src=\"https:\/\/discover.restek.com\/wp-content\/uploads\/\/figure-article-FSSS3549-01-790x1024.jpg\" alt=\"\" class=\"wp-image-20259\" title=\"-\" srcset=\"https:\/\/discover.restek.com\/wp-content\/uploads\/figure-article-FSSS3549-01-790x1024.jpg 790w, https:\/\/discover.restek.com\/wp-content\/uploads\/figure-article-FSSS3549-01-231x300.jpg 231w, https:\/\/discover.restek.com\/wp-content\/uploads\/figure-article-FSSS3549-01-768x996.jpg 768w, https:\/\/discover.restek.com\/wp-content\/uploads\/figure-article-FSSS3549-01-1185x1536.jpg 1185w, https:\/\/discover.restek.com\/wp-content\/uploads\/figure-article-FSSS3549-01-1579x2048.jpg 1579w, https:\/\/discover.restek.com\/wp-content\/uploads\/figure-article-FSSS3549-01.jpg 1800w\" sizes=\"auto, (max-width: 790px) 100vw, 790px\" \/><\/figure>\n\n<\/div><\/div><\/div>\n\n\n<div style=\"height:50px\" aria-hidden=\"true\" class=\"wp-block-spacer\"><\/div>\n\n\n\n<h2 class=\"wp-block-heading\">Revive\u30a4\u30f3\u30e9\u30a4\u30f3\u30b5\u30f3\u30d7\u30eb\u524d\u51e6\u7406\u306e\u3057\u304f\u307f<\/h2>\n\n\n\n<p>\u56f32\u306b\u793a\u3059\u3088\u3046\u306b\u3001Revive ILSP\u306f\u3001\u30b5\u30f3\u30d7\u30eb\u30af\u30ea\u30fc\u30f3\u30a2\u30c3\u30d7\u30ab\u30fc\u30c8\u30ea\u30c3\u30b8\u3092LC\u306e\u6ce8\u5165\u6d41\u8def\u306b\u76f4\u63a5\u7d44\u307f\u8fbc\u3093\u3067\u3044\u307e\u3059\u3002\u5206\u6790\u7a2e\u304c\u5206\u6790\u30ab\u30e9\u30e0\u306b\u5230\u9054\u3059\u308b\u3068\u3001ILSP\u30af\u30ea\u30fc\u30f3\u30a2\u30c3\u30d7\u30ab\u30fc\u30c8\u30ea\u30c3\u30b8\u306f\u3001\u305d\u306e\u5f8c\u3001\u30d0\u30c3\u30af\u30d5\u30e9\u30c3\u30b7\u30e5\u307e\u305f\u306f\u300c\u518d\u751f\u300d\u3055\u308c\u3001\u6700\u521d\u306e\u30b5\u30f3\u30d7\u30eb\u3092\u5206\u6790\u4e2d\u306b\u6b21\u306e\u6ce8\u5165\u306b\u5099\u3048\u307e\u3059\u30026\u30dd\u30fc\u30c8\u30d0\u30eb\u30d6\u3068\u6a19\u6e96\u30bf\u30a4\u30d7\u306e\u72ec\u7acb\u3057\u305f\u30a4\u30bd\u30af\u30e9\u30c6\u30a3\u30c3\u30af\u30dd\u30f3\u30d7\u3092\u4f7f\u7528\u3059\u308b\u3053\u3068\u3067\u3001\u518d\u751f\u3068\u5206\u6790\u3092\u540c\u6642\u306b\u304a\u3053\u306a\u3046\u3053\u3068\u304c\u3067\u304d\u307e\u3059\u3002\u30b7\u30b9\u30c6\u30e0\u69cb\u6210\u3001\u30e1\u30bd\u30c3\u30c9\u30d1\u30e9\u30e1\u30fc\u30bf\u306e\u8a2d\u5b9a(\u4f8b\u3048\u3070\u3001\u30d0\u30eb\u30d6\u5207\u308a\u66ff\u3048\u306e\u30bf\u30a4\u30df\u30f3\u30b0\u3084\u6d17\u6d44\u6eb6\u5a92\u6d41\u91cf)\u3001\u304a\u3088\u3073\u52b9\u679c\u7684\u306a\u6d17\u6d44\u6eb6\u5a92\u306e\u7279\u5b9a\u306b\u95a2\u3059\u308b\u30ac\u30a4\u30c0\u30f3\u30b9\u306f\u3001Restek\u306eILSP\u30e1\u30bd\u30c3\u30c9\u958b\u767a\u30ac\u30a4\u30c9\u30e9\u30a4\u30f3\u306b\u8a18\u8f09\u3055\u308c\u3066\u3044\u307e\u3059\u3002\u7279\u306b\u5927\u91cf\u306e\u30b5\u30f3\u30d7\u30eb\u3092\u51e6\u7406\u3059\u308b\u30e9\u30dc\u3084\u30b5\u30f3\u30d7\u30eb\u524d\u51e6\u7406\u306e\u30ea\u30bd\u30fc\u30b9\u304c\u9650\u3089\u308c\u3066\u3044\u308b\u30e9\u30dc\u306b\u3068\u3063\u3066\u3001\u30dd\u30f3\u30d7\u3084\u30e1\u30bd\u30c3\u30c9\u30bb\u30c3\u30c8\u30a2\u30c3\u30d7\u306b\u8cbb\u3084\u3059\u6642\u9593\u3068\u3044\u3063\u305f\u6295\u8cc7\u306f\u3001\u65e5\u3005\u306e\u904b\u7528\u30b3\u30b9\u30c8\u306e\u4f4e\u6e1b\u3067\u307e\u304b\u306a\u3048\u308b\u306e\u3067\u306f\u306a\u3044\u3067\u3057\u3087\u3046\u304b\u3002<\/p>\n\n\n<div class=\"wp-block-custom-chromatogram-article-top\"><div class=\"chromatogram-article-placeholder\"><div class=\"figure-heading\"><strong>\u56f3 2:<\/strong>\u00a0\u30a4\u30f3\u30e9\u30a4\u30f3\u30b5\u30f3\u30d7\u30eb\u524d\u51e6\u7406\u306e\u3057\u304f\u307f<\/div><div class='chromatogram-article-inner-full'><div class=\"chromatogram-article-inner\">\n\n<figure class=\"wp-block-image size-large\"><img loading=\"lazy\" decoding=\"async\" width=\"1024\" height=\"897\" src=\"https:\/\/discover.restek.com\/wp-content\/uploads\/\/figure-article-FSSS3549-02-1024x897.jpg\" alt=\"\" class=\"wp-image-20271\" title=\"-\" srcset=\"https:\/\/discover.restek.com\/wp-content\/uploads\/figure-article-FSSS3549-02-1024x897.jpg 1024w, https:\/\/discover.restek.com\/wp-content\/uploads\/figure-article-FSSS3549-02-300x263.jpg 300w, https:\/\/discover.restek.com\/wp-content\/uploads\/figure-article-FSSS3549-02-768x672.jpg 768w, https:\/\/discover.restek.com\/wp-content\/uploads\/figure-article-FSSS3549-02-1536x1345.jpg 1536w, https:\/\/discover.restek.com\/wp-content\/uploads\/figure-article-FSSS3549-02.jpg 1800w\" sizes=\"auto, (max-width: 1024px) 100vw, 1024px\" \/><\/figure>\n\n<\/div><\/div><\/div>\n\n\n<div style=\"height:50px\" aria-hidden=\"true\" class=\"wp-block-spacer\"><\/div>\n\n\n\n<h2 class=\"wp-block-heading\">\u9ad8\u3044\u8010\u4e45\u6027\u3068\u305d\u306e\u9593\u306e\u4e00\u8cab\u3057\u305f\u7d50\u679c\u304c\u793a\u3059\u8cbb\u7528\u5bfe\u52b9\u679c<\/h2>\n\n\n\n<p>\u30a2\u30dc\u30ab\u30c9\u62bd\u51fa\u6db2\u306e300\u56de\u6ce8\u5165\u306b\u3088\u308b\u8010\u4e45\u6027\u5b9f\u9a13\u306f\u3001\u6642\u9593\u306e\u77ed\u7e2e\u306b\u52a0\u3048\u3001ILSP\u304c\u3082\u305f\u3089\u3059\u4e00\u8cab\u3057\u305f\u7d50\u679c\u3068\u5927\u5e45\u306a\u30b3\u30b9\u30c8\u524a\u6e1b\u306e\u512a\u308c\u305f\u4f8b\u3092\u63d0\u4f9b\u3057\u307e\u3059\u3002\u8102\u8cea\u306e\u591a\u3044\u30a2\u30dc\u30ac\u30c9\u306b\u3001\u5316\u5b66\u7684\u7279\u6027\u304a\u3088\u3073\u4fdd\u6301\u6642\u9593\u304c\u7570\u306a\u308b61\u7a2e\u985e\u306e\u4ee3\u8868\u7684\u306a\u6df7\u5408\u8fb2\u85ac\u3092\u6dfb\u52a0\u3057\u307e\u3057\u305f\u3002\u6b21\u3044\u3067\u3001\u56f33\u306b\u793a\u3059\u6700\u9069\u5316\u3055\u308c\u305f\u30ef\u30fc\u30af\u30d5\u30ed\u30fc\u3092\u7528\u3044\u3066\u30b5\u30f3\u30d7\u30eb\u3092\u62bd\u51fa\u304a\u3088\u3073\u5206\u6790\u3057\u307e\u3057\u305f\u3002\u30a4\u30f3\u30e9\u30a4\u30f3\u30b5\u30f3\u30d7\u30eb\u524d\u51e6\u7406\u6cd5\u306f\u3001\u540c\u7b49\u306eQuEChERS\u30a2\u30dc\u30ab\u30c9\u30ef\u30fc\u30af\u30d5\u30ed\u30fc\u3088\u308a\u3082\u5927\u5e45\u306b\u8fc5\u901f\u3067\u3001Revive ILSP\u8fb2\u85ac\u30ab\u30fc\u30c8\u30ea\u30c3\u30b81\u500b\u3067\u3001\u5b9f\u9a13\u671f\u9593\u306b\u308f\u305f\u3063\u3066\u52b9\u679c\u7684\u306a\u30af\u30ea\u30fc\u30f3\u30a2\u30c3\u30d7\u3068\u4e00\u8cab\u3057\u305f\u30af\u30ed\u30de\u30c8\u30b0\u30e9\u30d5\u30a3\u30fc\u7d50\u679c\u3092\u63d0\u4f9b\u3057\u307e\u3057\u305f\u3002<\/p>\n\n\n<div class=\"wp-block-custom-chromatogram-article-top\"><div class=\"chromatogram-article-placeholder\"><div class=\"figure-heading\"><strong>\u56f3 3:<\/strong>\u00a0\u8102\u8cea\u542b\u6709\u91cf\u306e\u9ad8\u3044\u30a2\u30dc\u30ab\u30c9\u30b5\u30f3\u30d7\u30eb\u306b\u304a\u3051\u308b\u30a4\u30f3\u30e9\u30a4\u30f3\u30b5\u30f3\u30d7\u30eb\u524d\u51e6\u7406\u306e\u30ef\u30fc\u30af\u30d5\u30ed\u30fc\u4f8b<\/div><div class='chromatogram-article-inner-full'><div class=\"chromatogram-article-inner\">\n\n<figure class=\"wp-block-image size-large\"><img loading=\"lazy\" decoding=\"async\" width=\"1024\" height=\"922\" src=\"https:\/\/discover.restek.com\/wp-content\/uploads\/\/figure-article-FSSS3549-03-1024x922.jpg\" alt=\"\" class=\"wp-image-20283\" title=\"-\" srcset=\"https:\/\/discover.restek.com\/wp-content\/uploads\/figure-article-FSSS3549-03-1024x922.jpg 1024w, https:\/\/discover.restek.com\/wp-content\/uploads\/figure-article-FSSS3549-03-300x270.jpg 300w, https:\/\/discover.restek.com\/wp-content\/uploads\/figure-article-FSSS3549-03-768x691.jpg 768w, https:\/\/discover.restek.com\/wp-content\/uploads\/figure-article-FSSS3549-03-1536x1382.jpg 1536w, https:\/\/discover.restek.com\/wp-content\/uploads\/figure-article-FSSS3549-03.jpg 1800w\" sizes=\"auto, (max-width: 1024px) 100vw, 1024px\" \/><\/figure>\n\n<\/div><\/div><\/div>\n\n\n<div style=\"height:50px\" aria-hidden=\"true\" class=\"wp-block-spacer\"><\/div>\n\n\n\n<p>\u56f34\u3067\u3068\u308a\u3042\u3052\u3066\u3044\u308b3\u3064\u306e\u8fb2\u85ac\u306f\u3001\u5206\u6790\u7a2e\u30ea\u30b9\u30c8\u5168\u4f53\u306e\u3046\u3061\u6eb6\u51fa\u304c\u65e9\u3044\u3001\u4e2d\u7a0b\u5ea6\u306e\u305d\u3057\u3066\u9045\u3044\u5316\u5408\u7269\u3067\u3059\u3002\u6570\u767e\u56de\u306e\u30de\u30c8\u30ea\u30c3\u30af\u30b9\u6ce8\u5165\u306e\u9593\u3067\u306e\u4e00\u8cab\u3057\u305f\u4fdd\u6301\u6642\u9593\u3001\u30d4\u30fc\u30af\u5f62\u72b6\u3001\u304a\u3088\u3073\u30ec\u30b9\u30dd\u30f3\u30b9\u306f\u3001Revive ILSP \u8fb2\u85ac\u30ab\u30fc\u30c8\u30ea\u30c3\u30b8\u306b\u3088\u308b\u30af\u30ea\u30fc\u30f3\u30a2\u30c3\u30d7\u306e\u9811\u5065\u6027\u3092\u5b9f\u8a3c\u3057\u307e\u3059\u3002\u540c\u3058\u62bd\u51fa\u6db2\u3092n=3\u3067\u6ce8\u5165\u3057\u3066\u8a55\u4fa1\u3057\u305f\u3068\u3053\u308d\u3001\u30e2\u30cb\u30bf\u30fc\u3057\u305f61\u7a2e\u985e\u306e\u8fb2\u85ac\u306e\u3046\u3061\u300195\uff05\u306f\u3001EU\u30ea\u30d5\u30a1\u30ec\u30f3\u30b9\u30e9\u30dc\u30e9\u30c8\u30ea\u30fc\u30ba\u306eSANTE\/12682\/2019\u30ac\u30a4\u30c9\u30e9\u30a4\u30f3\u306b\u3088\u3063\u3066\u78ba\u7acb\u3055\u308c\u305f\u6027\u80fd\u30ac\u30a4\u30c9\u30e9\u30a4\u30f3\uff08\u56de\u53ce\u738770\uff5e120\uff05\u3001\uff05RSD\u226620\uff05\uff09\u3092\u6e80\u305f\u3057\u307e\u3057\u305f[2]\u3002<\/p>\n\n\n\n<p>\u30b9\u30d4\u30fc\u30c9\u306e\u5411\u4e0a\u3068\u5805\u7262\u306a\u6027\u80fd\u306b\u52a0\u3048\u3066\u3001ILSP\u306f\u5927\u5e45\u306a\u30b3\u30b9\u30c8\u524a\u6e1b\u3082\u63d0\u4f9b\u3057\u307e\u3059\u3002\u4f8b\u3048\u3070\u3001QuEChERS\u30b5\u30f3\u30d7\u30eb(\u62bd\u51fa\u5869\u30d1\u30b1\u30c3\u30c8\u3068dSPE\u30c1\u30e5\u30fc\u30d6)\u3067\u306f\u30011\u30b5\u30f3\u30d7\u30eb\u5f53\u305f\u308a4\u30c9\u30eb\u3068\u4eee\u5b9a\u3059\u308b\u3068\u3001300\u306e\u30a2\u30dc\u30ab\u30c9\u30b5\u30f3\u30d7\u30eb\u306e\u5834\u5408\u3001QuEChERS\u88fd\u54c1\u306e\u307f\u30671200\u30c9\u30eb\u306e\u8cbb\u7528\u304c\u304b\u304b\u308b\u3053\u3068\u306b\u306a\u308a\u307e\u3059\u3002Revive\u30a4\u30f3\u30e9\u30a4\u30f3\u30b5\u30f3\u30d7\u30eb\u524d\u51e6\u7406\u30ef\u30fc\u30af\u30d5\u30ed\u30fc\u306f\u3001\u62bd\u51fa\u5869\u307e\u305f\u306fdSPE\u3092\u4f7f\u308f\u305a\u306b\u7c21\u5358\u306a\u56fa\u6db2\u62bd\u51fa\u3092\u4f7f\u7528\u3057\u3066\u3001\u305d\u306e\u8cbb\u7528\u3092\u4f4e\u6e1b\u3057\u307e\u3059\u3002Revive ILSP \u8fb2\u85ac\u30ab\u30fc\u30c8\u30ea\u30c3\u30b81\u500b\u306f\u3001QuEChERS\u306e\u7dcf\u4fa1\u683c\u306e\u7d041\/4\u306e\u8cbb\u7528\u3067\u3059\u3002300\u306e\u30a2\u30dc\u30ab\u30c9\u30b5\u30f3\u30d7\u30eb\u3092\u52b9\u679c\u7684\u306b\u30af\u30ea\u30fc\u30f3\u30a2\u30c3\u30d7\u3057\u3001\u305d\u306e\u6027\u80fd\u306f300\u56de\u6ce8\u5165\u5f8c\u3067\u3082\u4f4e\u4e0b\u3057\u306a\u304b\u3063\u305f\u305f\u3081\u3001\u5b9f\u9a13\u304c\u7d42\u4e86\u3057\u305f\u969b\u306b\u30ab\u30fc\u30c8\u30ea\u30c3\u30b8\u3092\u4ea4\u63db\u3059\u308b\u5fc5\u8981\u306f\u3042\u308a\u307e\u305b\u3093\u3067\u3057\u305f\u3002<\/p>\n\n\n<div class=\"wp-block-custom-chromatogram-article-top\"><div class=\"chromatogram-article-placeholder\"><div class=\"figure-heading\"><strong>\u56f3 4:<\/strong>\u00a01\u3064\u306eRevive ILSP\u30ab\u30fc\u30c8\u30ea\u30c3\u30b8\u306b300\u56de\u30a2\u30dc\u30ab\u30c9\u30de\u30c8\u30ea\u30c3\u30af\u30b9\u3092\u6ce8\u5165\u3057\u305f\u5f8c\u3067\u3082\u30af\u30ed\u30de\u30c8\u30b0\u30e9\u30d5\u30a3\u30fc\u306f\u5b89\u5b9a\u3057\u3066\u3044\u307e\u3059\u3002\u00a0<\/div><div class='chromatogram-article-inner-full'><div class=\"chromatogram-article-inner\">\n<div class=\"wp-block-custom-chromatogram-article\"><div class=\"wp-block-custom-chromatogram-article\"><div class=\"chromatogram-image regular-image\"><img decoding=\"async\" src=\"https:\/\/ez.restek.com\/images\/cgram\/lc_ff0584.png\" alt=\"ILSP Lifetime Study with Avocado\" title=\"-\"><\/div><p class=\"article-id\" style=\"text-align:center\"> LC_FF0584<\/p><div class=\"chromatogram-peaks\"><h4>Peaks<\/h4><table class=\"peaks col-lg-6 col-12\">\n<thead><tr><th><\/th><th style=\"text-align: left;width: 75px\">Peaks<\/th><th style=\"text-align: center;width: 75px\">t<sub>R<\/sub> (min)<\/th><th style=\"text-align: center;width: 75px\">Conc.<br \/>(ng\/g)<\/th><th style=\"text-align: center;width: 75px\">Precursor Ion<\/th><th style=\"text-align: center;width: 75px\">Product Ion 1<\/th><th style=\"text-align: center;width: 75px\">Product Ion 2<\/th><\/tr><\/thead>\n<tbody><tr><td class=\"num\">1.<\/td><td class=\"cmpd\"><a class=\"cmpd_link\" title=\"View compound information for Imidacloprid\" href=\"https:\/\/ez.restek.com\/compound\/view\/en\/138261-41-3\/Imidacloprid\" target=\"_blank\" rel=\"noopener\">Imidacloprid<\/a><\/td><td class=\"oth\">2.678<\/td><td class=\"oth\">50<\/td><td class=\"oth\">256.1<\/td><td class=\"oth\">175.0<\/td><td class=\"oth\">209.0<\/td><\/tr>\n<tr><td class=\"num\">2.<\/td><td class=\"cmpd\"><a class=\"cmpd_link\" title=\"View compound information for Fenhexamid\" href=\"https:\/\/ez.restek.com\/compound\/view\/en\/126833-17-8\/Fenhexamid\" target=\"_blank\" rel=\"noopener\">Fenhexamid<\/a><\/td><td class=\"oth\">4.557<\/td><td class=\"oth\">50<\/td><td class=\"oth\">302.1<\/td><td class=\"oth\">97.1<\/td><td class=\"oth\">55.05<\/td><\/tr>\n<tr><td class=\"num\">3.<\/td><td class=\"cmpd\"><a class=\"cmpd_link\" title=\"View compound information for Eprinomectin\" href=\"https:\/\/ez.restek.com\/compound\/view\/en\/123997-26-2\/Eprinomectin\" target=\"_blank\" rel=\"noopener\">Eprinomectin<\/a><\/td><td class=\"oth\">6.396<\/td><td class=\"oth\">50<\/td><td class=\"oth\">914.6<\/td><td class=\"oth\">186.1<\/td><td class=\"oth\">154.1<\/td><\/tr>\n<\/tbody><\/table><\/div><div class=\"chromatogram-conditions\"><h4>Conditions<\/h4><div class=\"conditions-container container-fluid\"><div class=\"row\"><table class=\"conditions col-lg-6 col-12\"><tr><th class=\"conditions_header\" scope=\"row\">Column<\/th><td>Raptor ARC-18  (<a target=\"_blank\" href=\"https:\/\/www.restek.com\/p\/9314A12?utm_source=chromatograms&amp;utm_medium=link&amp;utm_campaign=LC_FF0584\" rel=\"noopener\">cat.# 9314A12<\/a>)<\/td><\/tr><tr><th class=\"sub conditions_header\" scope=\"row\">Dimensions:<\/th><td>100 mm x 2.1 mm ID<\/td><\/tr><tr><th class=\"sub conditions_header\" scope=\"row\">Particle Size:<\/th><td>2.7 \u00b5m<\/td><\/tr><tr><th class=\"sub conditions_header\" scope=\"row\">Pore Size:<\/th><td>90 \u00c5<\/td><\/tr><tr><td><\/td><tr><th class=\"sub conditions_header\" scope=\"row\">Guard Column:<\/th><td>Raptor ARC-18 EXP guard column cartridge 5 mm, 2.1 mm ID, 2.7 \u00b5m (<a target=\"_blank\" href=\"https:\/\/www.restek.com\/p\/9314A0252?utm_source=chromatograms&amp;utm_medium=link&amp;utm_campaign=LC_FF0584\" rel=\"noopener\">cat.# 9314A0252<\/a>)<\/td><\/tr><tr><th class=\"sub conditions_header\" scope=\"row\">Temp.:<\/th><td>50 \u00b0C<\/td><\/tr><tr class=\"cgram_header_row\"><th class=\"conditions_header\" scope=\"row\">Standard\/Sample<\/th><td><\/td><\/tr><tr><th class=\"sub conditions_header\" scope=\"row\">Diluent:<\/th><td>Acetonitrile, 0.1% acetic acid<\/td><\/tr><td><\/td><\/tr><tr><th class=\"sub conditions_header\" scope=\"row\">Inj. Vol.:<\/th><td>3 \u00b5L <\/td><\/tr><tr class=\"cgram_header_row\"><th class=\"conditions_header\" scope=\"row\">Mobile Phase<\/th><td><\/td><\/tr><tr><th class=\"sub conditions_header\" scope=\"row\">A:<\/th><td>Water, 0.2% formic acid, 2 mM ammonium formate <\/td><\/tr><tr><th class=\"sub conditions_header\" scope=\"row\">B:<\/th><td>Methanol, 0.2% formic acid, 2 mM ammonium formate <\/td><\/tr><tr><th class=\"sub conditions_header\" scope=\"row\">C:<\/th><td>Methanol, 0.2% formic acid, 10 mM ammonium formate <\/td><\/tr><tr><td><\/td><td><table class=\"cgram_ramp\"><thead><tr><th>Time (min)<\/th><th>Flow (mL\/min)<\/th><th>%A<\/th><th>%B<\/th><\/tr><\/thead><tbody><tr><td>0.00<\/td><td>0.4<\/td><td>95<\/td><td>5<\/td><\/tr><tr><td>2<\/td><td>0.4<\/td><td>40<\/td><td>60<\/td><\/tr><tr><td>4<\/td><td>0.4<\/td><td>25<\/td><td>75<\/td><\/tr><tr><td>6<\/td><td>0.4<\/td><td>0<\/td><td>100<\/td><\/tr><tr><td>8<\/td><td>0.4<\/td><td>0<\/td><td>100<\/td><\/tr><tr><td>8.01<\/td><td>0.4<\/td><td>95<\/td><td>5<\/td><\/tr><tr><td>10<\/td><td>0.4<\/td><td>95<\/td><td>5<\/td><\/tr><\/tbody><\/table><\/td><\/tr><\/table><table class=\"conditions col-lg-6 col-12\"><tr><th class=\"conditions_header\" scope=\"row\">Detector<\/th><td>MS\/MS<\/td><\/tr><tr><th class=\"sub conditions_header\" scope=\"row\">Ion Source:<\/th><td>Electrospray <\/td><\/tr><tr><th class=\"sub conditions_header\" scope=\"row\">Ion Mode:<\/th><td>ESI+ <\/td><\/tr><tr><th class=\"sub conditions_header\" scope=\"row\">Mode:<\/th><td>MRM <\/td><\/tr><tr class=\"cgram_header_row\"><th class=\"conditions_header\" scope=\"row\">Instrument<\/th><td>UHPLC<\/td><\/tr><tr class=\"cgram_header_row\"><th class=\"conditions_header\" scope=\"row\">Sample Preparation<\/th><td><i>Sample Fortification and Extraction<\/i><br \/>Avocado was peeled and homogenized, and 5 g of sample was weighed into a 50 mL polypropylene tube. 10 mL of acetonitrile containing 0.1% acetic acid was added to the sample and vortexed. Samples were shaken on a shaker table for 10 minutes and then centrifuged at 4200 rpm for 10 minutes. An aliquot was transferred to a vial and fortified with analytes for a final concentration of 50 ng\/g. The sample was vortexed, and an aliquot transferred to a 0.2 \u03bcm PTFE Thomson filter vial cat.# 25893 and filtered prior to injection. <br \/><br \/><i>In-Line Sample Preparation (ILSP)<\/i><br \/>The UHPLC system was equipped with an auxiliary pump; 6-port, high-pressure switching valve; and dual-directional 5 x 2.1 mm Revive ILSP Pesticides cartridge and holder (<a target=\"_blank\" href=\"https:\/\/www.restek.com\/p\/27882?utm_source=chromatograms&amp;utm_medium=link&amp;utm_campaign=LC_FF0584\" rel=\"noopener\">cat.# 27882<\/a>). At 5.5 min, after the target compounds had all eluted from the ILSP cartridge and were undergoing analysis, valve switching was used as described below to flush the ILSP cartridge and wash trapped matrix components to waste. At 7.0 min, the original valve configuration, where the ILSP cartridge is in-line with the analytical column, was restored and the system was brought back to equilibrium prior to the next injection.<br \/>\u2022 0 min; valve position 0<br \/>\u2022 0 min; C flow= 0 mL\/min<br \/>\u2022 5.49 min; C flow= 0 mL\/min<br \/>\u2022 5.5 min; valve position 1<br \/>\u2022 5.5 min; C flow= 1 mL\/min<br \/>\u2022 6.9 min; C flow=1 mL\/min<br \/>\u2022 7 min; C flow= 0 mL\/min<br \/>\u2022 7 min; valve position 0<br \/><br \/><\/td><\/tr><tr class=\"cgram_header_row\"><th class=\"conditions_header\" scope=\"row\">Notes<\/th><td>Thomson SINGLE StEP standard filter vials cat.# 25893 were used to produce this chromatogram, but have since been discontinued. For assistance choosing a replacement for this application, contact Restek Technical Service or your local Restek representative.<br \/><\/td><\/tr><\/table><\/div><\/div><\/div><div class=\"chromatogram-pdf-link\"><a href=\"https:\/\/ez.restek.com\/images\/cgram\/lc_ff0584.pdf\" target=\"_blank\" rel=\"noopener noreferrer\"><svg xmlns=\"http:\/\/www.w3.org\/2000\/svg\" width=\"18\" height=\"18\" viewBox=\"0 0 18 18\"><g data-name=\"Group 2996\"><path data-name=\"Rectangle 1246\" d=\"M0 0h18v18H0z\" style=\"fill: none;\"><\/path><\/g><g data-name=\"Group 2997\"><path data-name=\"Path 729\" d=\"M13.412 11.4v2.017H5.345V11.4H4v2.017a1.349 1.349 0 0 0 1.345 1.345h8.068a1.349 1.349 0 0 0 1.345-1.345V11.4zm-.672-2.694-.948-.948-1.741 1.735V4H8.706v5.493L6.965 7.758l-.948.948 3.361 3.361z\" transform=\"translate(-.437 -.414)\" style=\"fill: rgb(13, 123, 196);\"><\/path><\/g><\/svg>Download PDF<\/a><\/div><\/div><\/div>\n<\/div><\/div><\/div>\n\n\n<div style=\"height:50px\" aria-hidden=\"true\" class=\"wp-block-spacer\"><\/div>\n\n\n\n<h2 class=\"wp-block-heading\">Revive ILSP\u5206\u6790\u4f8b: \u6027\u8cea\u306e\u7570\u306a\u308b\u98df\u54c1\u306b\u304a\u3051\u308b\u591a\u6210\u5206\u6b8b\u7559\u8fb2\u85ac\u5206\u6790<\/h2>\n\n\n\n<p>\u98df\u54c1\u4e2d\u306e\u8fb2\u85ac\u5206\u6790\u306f\u3001\u5206\u6790\u7269\u306e\u5316\u5b66\u7684\u6027\u8cea\u304a\u3088\u3073\u30de\u30c8\u30ea\u30c3\u30af\u30b9\u306e\u7a2e\u985e(\u8102\u8cea\u304c\u591a\u3044\u3001\u7cd6\u8cea\u304c\u591a\u3044\u3001\u8272\u7d20\u304c\u591a\u3044\u3001\u6c34\u5206\u304c\u5c11\u306a\u3044\u306a\u3069)\u304c\u5e45\u5e83\u3044\u305f\u3081\u3001\u7279\u306b\u56f0\u96e3\u3067\u3059\u3002\u3053\u308c\u306b\u5bfe\u51e6\u3059\u308b\u305f\u3081\u306b\u3001\u3055\u307e\u3056\u307e\u306aQuEChERS\u88fd\u54c1\u304c\u7528\u610f\u3055\u308c\u3066\u304a\u308a\u3001\u7570\u306a\u308b\u72b6\u6cc1\u306b\u304a\u3044\u3066\u3082\u52b9\u679c\u7684\u306a\u62bd\u51fa\u3068\u30af\u30ea\u30fc\u30f3\u30ca\u30c3\u30d7\u3092\u78ba\u5b9f\u306a\u3082\u306e\u3068\u3057\u3066\u3044\u307e\u3059\u3002\u3057\u304b\u3057\u30011\u3064\u306eRevive ILSP \u8fb2\u85ac\u30ab\u30fc\u30c8\u30ea\u30c3\u30b8\u306f\u3001\u540c\u3058\u5e83\u7bc4\u56f2\u306e\u5206\u6790\u7a2e\u304a\u3088\u3073\u30de\u30c8\u30ea\u30c3\u30af\u30b9\u306b\u308f\u305f\u3063\u3066\u512a\u308c\u305f\u7d50\u679c\u3092\u63d0\u4f9b\u3059\u308b\u3053\u3068\u304c\u3067\u304d\u307e\u3059\u3002&nbsp;<\/p>\n\n\n\n<p>\u3053\u306e\u5e83\u7bc4\u306a\u9069\u7528\u6027\u3092\u793a\u3059\u305f\u3081\u306b\u3001SANTE\/12682\/2019\u30ac\u30a4\u30c9\u30e9\u30a4\u30f3\u306e5\u3064\u306e\u98df\u54c1\u30b0\u30eb\u30fc\u30d7\u306b\u307e\u305f\u304c\u308b6\u3064\u306e\u98df\u54c1\u306b\u5bfe\u3057\u3001\u958b\u767a\u3055\u308c\u305f\u30a4\u30f3\u30e9\u30a4\u30f3\u30b5\u30f3\u30d7\u30eb\u524d\u51e6\u7406\u65b9\u6cd5\u3092\u4f7f\u7528\u3057\u3066\u56de\u53ce\u7387\u5b9f\u9a13\u3092\u304a\u3053\u306a\u3044\u307e\u3057\u305f(\u8868I)\u3002\u3053\u3053\u3067\u4f7f\u7528\u3057\u305f\u98df\u54c1\u306b\u306f\u3001\u4e00\u822c\u7684\u306a\u591a\u6210\u5206\u6b8b\u7559\u8fb2\u85ac\u30b9\u30af\u30ea\u30fc\u30cb\u30f3\u30b0\u30e1\u30bd\u30c3\u30c9\u306e\u30af\u30ed\u30de\u30c8\u30b0\u30e9\u30e0\u306b\u304a\u3044\u3066\u3001\u7570\u306a\u308b\u6642\u9593(\u65e9\u671f\u3001\u4e2d\u671f\u3001\u5f8c\u671f)\u306b\u6eb6\u51fa\u3059\u308b\u3055\u307e\u3056\u307e\u306a\u5316\u5b66\u7684\u6027\u8cea\u3092\u6709\u3059\u308b61\u306e\u8fb2\u85ac\u3092\u6dfb\u52a0\u3057\u307e\u3057\u305f(\u8868II)\u3002&nbsp;<\/p>\n\n\n\n<h5 class=\"wp-block-heading\"><strong>\u8868 I:<\/strong>&nbsp;Revive ILSP\u30e1\u30bd\u30c3\u30c9\u958b\u767a\u306b\u4f7f\u7528\u3057\u305f\u98df\u54c1<\/h5>\n\n\n\n<figure class=\"wp-block-table\"><table style=\"border-width:1px\"><thead><tr><th class=\"has-text-align-left\" data-align=\"left\"><strong>\u98df\u54c1\u30b0\u30eb\u30fc\u30d7<\/strong><\/th><th class=\"has-text-align-left\" data-align=\"left\"><strong>\u98df\u54c1\u30b5\u30f3\u30d7\u30eb<\/strong><\/th><\/tr><\/thead><tbody><tr><td class=\"has-text-align-left\" data-align=\"left\">\u6c34\u5206\u542b\u91cf\u304c\u9ad8\u304f\u8272\u7d20\u304c\u8c4a\u5bcc<\/td><td class=\"has-text-align-left\" data-align=\"left\">\u30db\u30a6\u30ec\u30f3\u30bd\u30a6<\/td><\/tr><tr><td class=\"has-text-align-left\" data-align=\"left\">\u9178\u542b\u91cf\u3068\u6c34\u5206\u542b\u91cf\u304c\u8c4a\u5bcc<\/td><td class=\"has-text-align-left\" data-align=\"left\">\u30aa\u30ec\u30f3\u30b8(\u5168\u4f53)<\/td><\/tr><tr><td class=\"has-text-align-left\" data-align=\"left\">\u8102\u8cea\u542b\u91cf\u304c\u9ad8\u304f\u3001\u6c34\u5206\u542b\u91cf\u304c\u975e\u5e38\u306b\u4f4e\u3044<\/td><td class=\"has-text-align-left\" data-align=\"left\">\u5927\u8c46\u30df\u30fc\u30eb<\/td><\/tr><tr><td class=\"has-text-align-left\" data-align=\"left\">\u8102\u8cea\u542b\u91cf\u304c\u9ad8\u304f\u3001\u6c34\u5206\u542b\u91cf\u306f\u4e2d\u7a0b\u5ea6<\/td><td class=\"has-text-align-left\" data-align=\"left\">\u30a2\u30dc\u30ab\u30c9<\/td><\/tr><tr><td class=\"has-text-align-left\" data-align=\"left\" rowspan=\"2\">&#8220;\u96e3\u3057\u3044\u3082\u3057\u304f\u306f\u30e6\u30cb\u30fc\u30af\u306a\u98df\u54c1&#8221;<\/td><td class=\"has-text-align-left\" data-align=\"left\">\u30cf\u30a4\u30d3\u30b9\u30ab\u30b9\u30c6\u30a3\u30fc<\/td><\/tr><tr><td class=\"has-text-align-left\" data-align=\"left\">\u7d05\u8336<\/td><\/tr><\/tbody><\/table><\/figure>\n\n\n\n<h5 class=\"wp-block-heading\"><strong>\u8868 II:<\/strong>&nbsp;\u4e00\u822c\u7684\u306a\u591a\u6210\u5206\u6b8b\u7559\u8fb2\u85ac\u30b9\u30af\u30ea\u30fc\u30cb\u30f3\u30b0\u30e1\u30bd\u30c3\u30c9\u3067\u5316\u5b66\u7684\u7279\u6027\u3068\u6eb6\u51fa\u6642\u9593(\u65e9\u3044\u3001\u4e2d\u7a0b\u5ea6\u3001\u9045\u3044)\u306e\u4e21\u65b9\u304c\u7570\u306a\u308b61\u7a2e\u985e\u306e\u8fb2\u85ac\u3092\u4f7f\u7528\u3057\u3066\u3001Revive ILSP\u306e\u56de\u53ce\u7387\u8a66\u9a13\u3092\u5b9f\u65bd\u3057\u307e\u3057\u305f\u3002<\/h5>\n\n\n\n<figure class=\"wp-block-table\"><table class=\"has-fixed-layout\" style=\"border-width:1px\"><tbody><tr><td colspan=\"3\"><strong>\u30e2\u30cb\u30bf\u30fc\u8fb2\u85ac\u30ea\u30b9\u30c8<\/strong><\/td><\/tr><tr><td>Cyromazine<\/td><td>Flutolanil<\/td><td>Benzoximate<\/td><\/tr><tr><td>Dinotefuran<\/td><td>Mepronil<\/td><td>Trifloxystrobin<\/td><\/tr><tr><td>Nitenpyram<\/td><td>Myclobutanil<\/td><td>Metaflumizone<\/td><\/tr><tr><td>Imidacloprid<\/td><td>Methoxyfenozide<\/td><td>Fluazinam<\/td><\/tr><tr><td>Acetamiprid<\/td><td>Triadimefon<\/td><td>Tebufenpyrad<\/td><\/tr><tr><td>Oxadixyl<\/td><td>Mepanipyrim<\/td><td>Pyriproxyfen<\/td><\/tr><tr><td>Carbetamide<\/td><td>Fluoxastrobin<\/td><td>Piperonyl Butoxide<\/td><\/tr><tr><td>Pyracarbolid<\/td><td>Fenhexamid<\/td><td>Quinoxyfen<\/td><\/tr><tr><td>Secbumeton<\/td><td>Butafenacil<\/td><td>Amitraz<\/td><\/tr><tr><td>Prometon<\/td><td>Cyprodinil<\/td><td>Fenpyroximate<\/td><\/tr><tr><td>Terbumeton<\/td><td>Picoxystrobin<\/td><td>Eprinomectin<\/td><\/tr><tr><td>Ametryn<\/td><td>Rotenone<\/td><td>Abamectin B1a<\/td><\/tr><tr><td>Metalaxyl<\/td><td>Tebufenozide<\/td><td>Fenazaquin<\/td><\/tr><tr><td>Chlorantraniliprole<\/td><td>Dimoxystrobin<\/td><td>Doramectin<\/td><\/tr><tr><td>Pyrimethanil<\/td><td>Carfentrazone-ethyl +NH4<\/td><td>Ivermectin<\/td><\/tr><tr><td>Spiroxamine<\/td><td>Kresoxym-methyl<\/td><td>Moxidectin<\/td><\/tr><tr><td>Azoxystrobin<\/td><td>Zoxamide<\/td><td>Imazalil<\/td><\/tr><tr><td>Halofenozide<\/td><td>Famoxadone<\/td><td>Pymetrozine<\/td><\/tr><tr><td>Furalaxyl<\/td><td>Benalaxyl<\/td><td>Fludioxinol<\/td><\/tr><tr><td>Boscalid<\/td><td>Clofentezine<\/td><td>&nbsp;<\/td><\/tr><tr><td>Mandipropamid<\/td><td>Prochloraz<\/td><td>&nbsp;<\/td><\/tr><\/tbody><\/table><\/figure>\n\n\n\n<h3 class=\"wp-block-heading\">ILSP \u30b5\u30f3\u30d7\u30eb\u62bd\u51fa<\/h3>\n\n\n\n<p>Revive ILSP\u306e\u30ef\u30fc\u30af\u30d5\u30ed\u30fc\u306b\u304a\u3051\u308b\u62bd\u51fa\u3001\u3064\u307e\u308a\u30b5\u30f3\u30d7\u30eb\u306e\u30db\u30e2\u30b8\u30ca\u30a4\u30ba\u5f8c\u306e\u56fa\u6db2\u62bd\u51fa\u306f\u3001\u8abf\u67fb\u3057\u305f\u5168\u3066\u306e\u98df\u54c1\u3067\u826f\u597d\u306b\u6a5f\u80fd\u3057\u307e\u3057\u305f\u3002\u6b63\u78ba\u306a\u62bd\u51fa\u30d1\u30e9\u30e1\u30fc\u30bf(\u6eb6\u5a92\u3001\u5bb9\u91cf\u3001\u632f\u3068\u3046\u6642\u9593\u3001\u308d\u904e\u306a\u3069)\u306f\u98df\u54c1\u3054\u3068\u306b\u6700\u9069\u5316\u3057\u307e\u3057\u305f\u304c\u3001\u5168\u4f53\u7684\u306a\u624b\u9806\u306f\u30b7\u30f3\u30d7\u30eb\u304b\u3064\u8fc5\u901f\u3067\u52b9\u679c\u7684\u3067\u3057\u305f\u3002\u30db\u30e2\u30b8\u30ca\u30a4\u30ba\u3001\u6eb6\u5a92\u6dfb\u52a0\u3001\u64b9\u306f\u3093\u3001\u305d\u3057\u3066\u5fc5\u8981\u306b\u5fdc\u3058\u3066\u30b5\u30f3\u30d7\u30eb\u308d\u904e\u3092\u304a\u3053\u306a\u3044\u307e\u3057\u305f\u3002\u3055\u3089\u306b\u3001QuEChERS\u6cd5\u3067\u4e00\u822c\u7684\u306a\u5206\u6563\u578b\u30af\u30ea\u30fc\u30f3\u30a2\u30c3\u30d7\u5de5\u7a0b\u304c\u306a\u3044\u305f\u3081\u3001\u30a4\u30f3\u30e9\u30a4\u30f3\u30b5\u30f3\u30d7\u30eb\u524d\u51e6\u7406\u30e1\u30bd\u30c3\u30c9\u306f\u3001\u30af\u30ea\u30fc\u30f3\u30a2\u30c3\u30d7\u4e2d\u306e\u5206\u6790\u7a2e\u306e\u30ed\u30b9\u3092\u6700\u5c0f\u9650\u306b\u6291\u3048\u307e\u3059\u3002<\/p>\n\n\n\n<h3 class=\"wp-block-heading\">\u3055\u307e\u3056\u307e\u306a\u98df\u54c1\u30b0\u30eb\u30fc\u30d7\u306b\u304a\u3051\u308bILSP\u306e\u56de\u53ce\u7387<\/h3>\n\n\n\n<p>\u8abf\u67fb\u3057\u305f\u8fb2\u85ac\u306e\u307b\u307c\u5168\u3066\u3092\uff16\u3064\u306e\u7570\u306a\u308b\u30de\u30c8\u30ea\u30c3\u30af\u30b9\u304b\u3089\u56de\u53ce\u3057\u3001\u305d\u306e\u56de\u53ce\u7387\u306f\u4f4e\uff5e\u4e2d\u7a0b\u5ea6\u306e\u611f\u5ea6\u3092\u6709\u3059\u308bLC-MS\/MS\u3092\u4f7f\u7528\u3057\u305fSANTE\/12682\/2019\u306b\u3088\u308b\u6027\u80fd\u30ac\u30a4\u30c9\u30e9\u30a4\u30f3\u306e\u7bc4\u56f2\u5185\u3067\u3057\u305f(\u8868III)\u3002\u3053\u308c\u3089\u306e\u7d50\u679c\u306f\u3001\u98df\u54c1\u3084\u98fc\u6599\u4e2d\u306e\u591a\u6210\u5206\u6b8b\u7559\u8fb2\u85ac\u30e2\u30cb\u30bf\u30ea\u30f3\u30b0\u306b\u304a\u3051\u308bRevive\u30a4\u30f3\u30e9\u30a4\u30f3\u30b5\u30f3\u30d7\u30eb\u524d\u51e6\u7406\u306e\u5e45\u5e83\u3044\u9069\u7528\u6027\u3092\u793a\u3057\u3066\u3044\u307e\u3059\u3002<\/p>\n\n\n\n<p>\u3055\u3089\u306b\u3001Revive ILSP\u3092\u985e\u4f3c\u306eQuEChERS\u6cd5\u3068\u6bd4\u8f03\u3057\u305f\u5834\u5408\u3001ILSP\u306f\u3001\u5168\u3066\u306e\u5834\u5408\u306b\u304a\u3044\u3066\u3001\u512a\u308c\u3066\u308b\u3068\u306f\u8a00\u3048\u306a\u3044\u307e\u3067\u3082\u3001\u540c\u7b49\u306e\u30d1\u30d5\u30a9\u30fc\u30de\u30f3\u30b9\u3092\u793a\u3057\u307e\u3057\u305f\u3002\u307e\u305f\u3001\u5316\u5408\u7269\u304c\u7406\u60f3\u7684\u306a70\uff5e120%\u306e\u56de\u53ce\u7387\u7bc4\u56f2\u3092\u5916\u308c\u305f\u5834\u5408\u3001ILSP\u306e\u81ea\u52d5\u5316\u3055\u308c\u305f\u518d\u73fe\u6027\u306e\u3042\u308b\u30af\u30ea\u30fc\u30f3\u30a2\u30c3\u30d7\u306e\u5834\u5408\u306e\u3088\u3046\u306b\u3001\u7d50\u679c\u304c\u4e00\u8cab\u3057\u3066\u3044\u308c\u3070\u3001SANTE\/12682\/2019\u306e\u3088\u3046\u306a\u30ac\u30a4\u30c9\u30e9\u30a4\u30f3\u306f\u3001\u305d\u306e\u30c7\u30fc\u30bf\u3092\u5831\u544a\u3059\u308b\u305f\u3081\u306e\u898f\u5b9a\u3092\u63d0\u4f9b\u3057\u3066\u3044\u307e\u3059\u3002&nbsp;<\/p>\n\n\n\n<h5 class=\"wp-block-heading\"><strong>\u8868 III:<\/strong>&nbsp;6\u3064\u306e\u7570\u306a\u308b\u98df\u54c1\u7528\u306b\u958b\u767a\u3057\u305fRevive ILSP\u30e1\u30bd\u30c3\u30c9\u306b\u3088\u308b\u5168\u4f53\u7684\u306a\u56de\u53ce\u7387\u6027\u80fd<\/h5>\n\n\n\n<figure class=\"wp-block-table\"><table style=\"border-width:1px\"><thead><tr><th class=\"has-text-align-left\" data-align=\"left\"><strong>\u98df\u54c1<\/strong><\/th><th class=\"has-text-align-left\" data-align=\"left\"><strong>&nbsp;\u56de\u53ce\u738770-120%\u3001&nbsp;RSD(\u6fc3\u5ea6)\u304c20%\u4ee5\u4e0b\u306e\u5316\u5408\u7269\u306e\u5272\u5408<\/strong><\/th><\/tr><\/thead><tbody><tr><td class=\"has-text-align-left\" data-align=\"left\">\u30db\u30a6\u30ec\u30f3\u30bd\u30a6<\/td><td class=\"has-text-align-left\" data-align=\"left\">85.7% (5 ng\/g); 95.2% (100 ng\/g)<\/td><\/tr><tr><td class=\"has-text-align-left\" data-align=\"left\">\u30aa\u30ec\u30f3\u30b8(\u5168\u4f53)<\/td><td class=\"has-text-align-left\" data-align=\"left\">87% (10 ng\/g)<\/td><\/tr><tr><td class=\"has-text-align-left\" data-align=\"left\">\u5927\u8c46\u30df\u30fc\u30eb<\/td><td class=\"has-text-align-left\" data-align=\"left\">97% (10 ng\/g)<\/td><\/tr><tr><td class=\"has-text-align-left\" data-align=\"left\">\u30a2\u30dc\u30ab\u30c9<\/td><td class=\"has-text-align-left\" data-align=\"left\">95% (10 ng\/g)<\/td><\/tr><tr><td class=\"has-text-align-left\" data-align=\"left\">\u30cf\u30a4\u30d3\u30b9\u30ab\u30b9\u30c6\u30a3\u30fc<\/td><td class=\"has-text-align-left\" data-align=\"left\">92% (10 ng\/g)<\/td><\/tr><tr><td class=\"has-text-align-left\" data-align=\"left\">\u7d05\u8336<\/td><td class=\"has-text-align-left\" data-align=\"left\">98% (10 ng\/g)<\/td><\/tr><\/tbody><\/table><\/figure>\n\n\n\n<h3 class=\"wp-block-heading\">\u30de\u30c8\u30ea\u30c3\u30af\u30b9\u52b9\u679c\u3068ILSP<\/h3>\n\n\n\n<p>\u5b9f\u969b\u306e\u30b5\u30f3\u30d7\u30eb\u306f\u3069\u306e\u3088\u3046\u306a\u5206\u6790\u306b\u304a\u3044\u3066\u3082\u3001\u4e00\u90e8\u306e\u30de\u30c8\u30ea\u30c3\u30af\u30b9\u306f\u76ee\u7684\u5316\u5408\u7269\u3068\u5171\u306b\u62bd\u51fa\u3055\u308c\u308b\u53ef\u80fd\u6027\u304c\u3042\u308a\u307e\u3059\u3002\u3053\u306e\u70b9\u306b\u95a2\u3057\u3066\u3001ILSP\u306f\u4ed6\u306e\u30b5\u30f3\u30d7\u30eb\u524d\u51e6\u7406\u6280\u8853\u3068\u5909\u308f\u3089\u305a\u3001\u30de\u30c8\u30ea\u30c3\u30af\u30b9\u30de\u30c3\u30c1\u691c\u91cf\u7dda\u7528\u6a19\u6e96\u6db2\u3092\u4f7f\u7528\u3059\u308b\u3053\u3068\u304c\u3001\u6b63\u78ba\u306a\u5b9a\u91cf\u3092\u4fdd\u8a3c\u3059\u308b\u305f\u3081\u306e\u6700\u826f\u306e\u65b9\u6cd5\u3067\u3059\u3002\u3053\u308c\u306f\u3001\u5206\u6790\u306e\u65e9\u3044\u6bb5\u968e\u3067\u6eb6\u51fa\u3059\u308b\u5316\u5408\u7269\u3067\u7279\u306b\u5f53\u3066\u306f\u307e\u308a\u307e\u3059\u3002\u4fdd\u6301\u3055\u308c\u306a\u3044\u30de\u30c8\u30ea\u30c3\u30af\u30b9\u6210\u5206\u304c\u6700\u3082\u73fe\u308c\u3084\u3059\u3044\u4f4d\u7f6e\u3067\u3042\u308a\u3001\u30a8\u30f3\u30cf\u30f3\u30b9\u30e1\u30f3\u30c8\u3042\u308b\u3044\u306f\u30b5\u30d7\u30ec\u30c3\u30b7\u30e7\u30f3\u3092\u5f15\u304d\u8d77\u3053\u3059\u53ef\u80fd\u6027\u304c\u3042\u308a\u307e\u3059\u3002<\/p>\n\n\n\n<p>\u5b9a\u91cf\u306b\u5f71\u97ff\u3092\u4e0e\u3048\u308b\u3060\u3051\u3067\u306a\u304f\u3001\u30de\u30c8\u30ea\u30c3\u30af\u30b9\u6210\u5206\u304c\u6a5f\u5668\u3092\u6c5a\u67d3\u3059\u308b\u53ef\u80fd\u6027\u304c\u3042\u308a\u307e\u3059\u3002\u30a4\u30f3\u30e9\u30a4\u30f3\u30b5\u30f3\u30d7\u30eb\u524d\u51e6\u7406\u6cd5\u3067\u306f\u3001\u672a\u7cbe\u88fd\u306e\u62bd\u51fa\u6db2\u3092\u6ce8\u5165\u3057\u307e\u3059\u3002\u30b5\u30f3\u30d7\u30eb\u9593\u306e\u30ad\u30e3\u30ea\u30fc\u30aa\u30fc\u30d0\u30fc\u3092\u56de\u907f\u3057\u3001\u53d6\u9664\u304f\u306e\u306b\u6a5f\u5668\u3092\u6b62\u3081\u308b\u3053\u3068\u304c\u5fc5\u8981\u3068\u306a\u308b\u3088\u3046\u306a\u6c5a\u67d3\u306e\u84c4\u7a4d\u3092\u9632\u3050\u305f\u3081\u3001\u6ce8\u5165\u6bce\u306b\u30cb\u30fc\u30c9\u30eb\u5185\u304a\u3088\u3073\u30cb\u30fc\u30c9\u30eb\u5916\u306e\u6d17\u6d44\u3092\u78ba\u5b9f\u306b\u304a\u3053\u306a\u3046\u3053\u3068\u304c\u91cd\u8981\u3067\u3059\u3002&nbsp;<\/p>\n\n\n\n<h2 class=\"wp-block-heading\">Revive\u30a4\u30f3\u30e9\u30a4\u30f3\u30b5\u30f3\u30d7\u30eb\u524d\u51e6\u7406: \u98df\u54c1\u4e2d\u306e\u591a\u6210\u5206\u6b8b\u7559\u8fb2\u85ac\u5206\u6790<\/h2>\n\n\n\n<p>\u30a4\u30f3\u30e9\u30a4\u30f3\u30b5\u30f3\u30d7\u30eb\u524d\u51e6\u7406\u306f\u3001LC-MS\/MS\u306e\u80fd\u529b\u3092\u4f7f\u7528\u3057\u3066\u3001\u30b5\u30f3\u30d7\u30eb\u62bd\u51fa\u7269\u30af\u30ea\u30fc\u30f3\u30a2\u30c3\u30d7\u3092\u52b9\u7387\u5316\u3057\u3001\u81ea\u52d5\u5316\u3057\u307e\u3059\u3002Revive ILSP \u8fb2\u85ac\u30ab\u30fc\u30c8\u30ea\u30c3\u30b8\u30016\u30dd\u30fc\u30c8\u30d0\u30eb\u30d6\u3001\u304a\u3088\u3073\u72ec\u7acb\u3057\u305f\u30a4\u30bd\u30af\u30e9\u30c6\u30a3\u30c3\u30af\u30dd\u30f3\u30d7\u3092\u4f7f\u7528\u3059\u308b\u3068\u3001\u30b5\u30f3\u30d7\u30eb\u306e\u30af\u30ea\u30fc\u30f3\u30a2\u30c3\u30d7\u3068\u5206\u96e2\u691c\u51fa\u3092\u4e00\u3064\u306e\u52b9\u7387\u7684\u306a\u65b9\u6cd5\u306b\u7d44\u5408\u308f\u305b\u3001\u6a5f\u5668\u3092\u5206\u6790\u306e\u4e3b\u529b\u3078\u3068\u5909\u3048\u308b\u3053\u3068\u304c\u3067\u304d\u307e\u3059\u3002Revive ILSP\u3092\u73fe\u5728\u306e\u98df\u54c1\u4e2d\u306e\u591a\u6210\u5206\u6b8b\u7559\u8fb2\u85ac\u5206\u6790\u30e1\u30bd\u30c3\u30c9\u306b\u7d71\u5408\u3059\u308b\u3053\u3068\u306b\u3088\u308a\u3001\u30b5\u30f3\u30d7\u30eb\u524d\u51e6\u7406\u6642\u9593\u3092\u77ed\u7e2e\u3057\u3001\u4f7f\u3044\u6368\u3066\u30b5\u30f3\u30d7\u30eb\u524d\u51e6\u7406\u88fd\u54c1\u306b\u307e\u3064\u308f\u308b\u30b3\u30b9\u30c8\u3092\u524a\u6e1b\u3057\u3001\u624b\u52d5\u624b\u9806\u306b\u95a2\u9023\u3057\u305f\u30a8\u30e9\u30fc\u3092\u4f4e\u6e1b\u3067\u304d\u307e\u3059\u3002<\/p>\n\n\n\n<h5 class=\"wp-block-heading\"><strong>\u53c2\u8003\u6587\u732e<\/strong><\/h5>\n\n\n\n<ol class=\"wp-block-list\">\n<li>A. Lupo, R.L. Romesberg, X. Lu, Automated inline pigment removal for the analysis of pesticide residues in spinach by liquid chromatography tandem mass spectrometry, J. Chromatogr. A 1629 (2020) 461477.&nbsp;<a href=\"https:\/\/doi.org\/10.1016\/j.chroma.2020.461477\" target=\"_blank\" rel=\"noreferrer noopener\">https:\/\/doi.org\/10.1016\/j.chroma.2020.461477<\/a><\/li>\n\n\n\n<li>EU Reference Laboratories for Residues of Pesticides, SANTE\/2019\/12682, Analytical quality control and method validation procedures for pesticide residues analysis in food and feed (2020).&nbsp;<a href=\"https:\/\/www.eurl-pesticides.eu\/userfiles\/file\/EurlALL\/AqcGuidance_SANTE_2019_12682.pdf\" target=\"_blank\" rel=\"noreferrer noopener\">https:\/\/www.eurl-pesticides.eu\/userfiles\/file\/EurlALL\/AqcGuidance_SANTE_2019_12682.pdf<\/a><\/li>\n<\/ol>\n\n\n\n<div style=\"height:100px\" aria-hidden=\"true\" class=\"wp-block-spacer\"><\/div>\n\n\n        <div class=\"cpb\">\n            <h3 class=\"cpb-heading\">Products Mentioned<\/h3>\n            <hr class=\"cpb-heading-underline\" \/>\n            <div class=\"cpb-list\">\n                                    <div class=\"cpb-item\">\n                        <div class=\"cpb-col cpb-col--left\">\n                            <a class=\"cpb-catalog\" target=\"_blank\" rel=\"noopener noreferrer\" href=\"https:\/\/www.restek.com\/p\/27882\">                                Catalog No. 27882                            <\/a>                        <\/div>\n                        <div class=\"cpb-col cpb-col--middle\">\n                            <div class=\"cpb-title\">Revive ILSP Holder and Revive ILSP Pesticides Cartridge, 5 x 2.1 mm<\/div>\n                        <\/div>\n                        <div class=\"cpb-col cpb-col--right\">\n                                                            <a class=\"cpb-view-btn\" target=\"_blank\" rel=\"noopener noreferrer\" href=\"https:\/\/www.restek.com\/p\/27882\">\u88fd\u54c1\u60c5\u5831\u3092\u898b\u308b<\/a>\n                                                    <\/div>\n                    <\/div>\n                                    <div class=\"cpb-item\">\n                        <div class=\"cpb-col cpb-col--left\">\n                            <a class=\"cpb-catalog\" target=\"_blank\" rel=\"noopener noreferrer\" href=\"https:\/\/www.restek.com\/p\/9314A12\">                                Catalog No. 9314A12                            <\/a>                        <\/div>\n                        <div class=\"cpb-col cpb-col--middle\">\n                            <div class=\"cpb-title\">Raptor ARC-18, 2.7 \u00b5m, 100 x 2.1 mm HPLC\u30ab\u30e9\u30e0<\/div>\n                        <\/div>\n                        <div class=\"cpb-col cpb-col--right\">\n                                                            <a class=\"cpb-view-btn\" target=\"_blank\" rel=\"noopener noreferrer\" href=\"https:\/\/www.restek.com\/p\/9314A12\">\u88fd\u54c1\u60c5\u5831\u3092\u898b\u308b<\/a>\n                                                    <\/div>\n                    <\/div>\n                                    <div class=\"cpb-item\">\n                        <div class=\"cpb-col cpb-col--left\">\n                            <a class=\"cpb-catalog\" target=\"_blank\" rel=\"noopener noreferrer\" href=\"https:\/\/www.restek.com\/p\/9314A0252\">                                Catalog No. 9314A0252                            <\/a>                        <\/div>\n                        <div class=\"cpb-col cpb-col--middle\">\n                            <div class=\"cpb-title\">Raptor ARC-18 EXP Guard Column Cartridge, 2.7 \u00b5m, 5 x 2.1 mm, 3-pk.<\/div>\n                        <\/div>\n                        <div class=\"cpb-col cpb-col--right\">\n                                                            <a class=\"cpb-view-btn\" target=\"_blank\" rel=\"noopener noreferrer\" href=\"https:\/\/www.restek.com\/p\/9314A0252\">\u88fd\u54c1\u60c5\u5831\u3092\u898b\u308b<\/a>\n                                                    <\/div>\n                    <\/div>\n                            <\/div>\n        <\/div>\n        \n\n\n<div style=\"height:100px\" aria-hidden=\"true\" class=\"wp-block-spacer\"><\/div>\n","protected":false},"excerpt":{"rendered":"<p>Revive in-line sample preparation combines an automated sample cleanup with concurrent analysis, significantly speeding up LC-MS\/MS multiresidue pesticide analysis in food.<\/p>\n","protected":false},"author":11,"featured_media":7068,"comment_status":"closed","ping_status":"open","sticky":false,"template":"","format":"standard","meta":{"_acf_changed":false,"_kad_blocks_custom_css":"","_kad_blocks_head_custom_js":"","_kad_blocks_body_custom_js":"","_kad_blocks_footer_custom_js":"","_kadence_starter_templates_imported_post":false,"_kad_post_transparent":"","_kad_post_title":"","_kad_post_layout":"","_kad_post_sidebar_id":"","_kad_post_content_style":"","_kad_post_vertical_padding":"","_kad_post_feature":"","_kad_post_feature_position":"","_kad_post_header":false,"_kad_post_footer":false,"footnotes":""},"categories":[789],"tags":[],"industries-application":[2275,2274],"post-badge":[],"resource-type":[],"product-library":[2581,2555],"resource-technique":[2343,2343],"hf_cat_post":[650],"ppma_author":[414],"class_list":["post-43628","post","type-post","status-publish","format-standard","has-post-thumbnail","hentry","category-articles-ja","industries-application-food-safety-ja","industries-application-food-beverage-ja","product-library-in-line-sample-preparation-ilsp-ja","product-library-sample-preparation-products-ja","resource-technique-liquid-chromatography-ja"],"acf":[],"taxonomy_info":{"category":[{"value":789,"label":"\u6280\u8853\u8cc7\u6599"}],"industries-application":[{"value":2275,"label":"\u98df\u306e\u5b89\u5168"},{"value":2274,"label":"\u98df\u54c1\uff5c\u98f2\u6599"}],"product-library":[{"value":2581,"label":"In-Line 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