{"id":43729,"date":"2025-10-03T21:35:58","date_gmt":"2025-10-03T21:35:58","guid":{"rendered":"https:\/\/discover.restek.com\/uncategorized\/fast-analysis-of-mcpds-by-lpgc-ms-japan\/"},"modified":"2026-01-21T19:31:41","modified_gmt":"2026-01-21T19:31:41","slug":"fast-analysis-of-mcpds-by-lpgc-ms-japan","status":"publish","type":"post","link":"https:\/\/discover.restek.com\/ja\/articles-ja\/gnfa4239-ja\/fast-analysis-of-mcpds-by-lpgc-ms-japan","title":{"rendered":"LPGC-MS\u306b\u3088\u308bMCPD\u306e\u9ad8\u901f\u5206\u6790"},"content":{"rendered":"\n<ul class=\"wp-block-list\">\n<li><strong>\u5f93\u6765\u306eGC-MS\u5206\u6790\u3088\u308a2\u500d\u306e\u5206\u6790\u30b9\u30d4\u30fc\u30c9<\/strong><\/li>\n\n\n\n<li><strong>\u5f93\u6765\u306eGC-MS\u6cd5\u3068\u6bd4\u8f03\u3057\u3066\u30d8\u30ea\u30a6\u30e0\u4f7f\u7528\u91cf\u309269\uff05\u524a\u6e1b<\/strong><\/li>\n\n\n\n<li><strong>Rxi-17Sil MS\u30ad\u30c3\u30c8\u306f\u3001\u51fa\u8377\u524d\u306b\u30ea\u30fc\u30af\u691c\u67fb\u3092\u5b9f\u65bd\u3057\u3066\u304a\u308a\u3001\u901a\u5e38\u306e\u30ad\u30e3\u30d4\u30e9\u30ea\u30fc\u30ab\u30e9\u30e0\u306e\u3088\u3046\u306b\u7c21\u5358\u306b\u53d6\u308a\u4ed8\u3051\u53ef\u80fd<\/strong><\/li>\n<\/ul>\n\n\n\n<p>MCPD\uff08\u30e2\u30ce\u30af\u30ed\u30ed\u30d7\u30ed\u30d1\u30f3\u30b8\u30aa\u30fc\u30eb\uff09\u306f\u98df\u54c1\u52a0\u5de5\u306e\u52a0\u71b1\u5de5\u7a0b\u3067\u751f\u6210\u3055\u308c\u308b\u53ef\u80fd\u6027\u304c\u3042\u308b\u5371\u967a\u306a\u4e0d\u7d14\u7269\u3067\u3042\u308a\u3001MCPD\u306b\u3064\u3044\u3066\u306e\u7814\u7a76\u3068\u691c\u51fa\u306f\u3001\u98df\u54c1\u5b89\u5168\u306b\u304a\u3051\u308b\u91cd\u8981\u306a\u8ab2\u984c\u3068\u306a\u3063\u3066\u3044\u307e\u3059\u3002\u7279\u306b\u690d\u7269\u6cb9\u3084\u30d1\u30fc\u30e0\u6cb9\u3068\u3044\u3063\u305f\u7cbe\u88fd\u6cb9\u304b\u3089\u3001\u3053\u306e\u7a2e\u306e\u4e0d\u7d14\u7269\u304c\u691c\u51fa\u3055\u308c\u308b\u3053\u3068\u304c\u591a\u304f\u3001\u307e\u305f\u3001\u3053\u308c\u3089\u7cbe\u88fd\u6cb9\u3092\u914d\u5408\u3057\u305f\u4e73\u5150\u7528\u7c89\u30df\u30eb\u30af\u306a\u3069\u306e\u52a0\u5de5\u98df\u54c1\u304b\u3089\u3082MCPD\u306f\u591a\u304f\u691c\u51fa\u3055\u308c\u307e\u3059\u3002MCPD\u306f\u901a\u5e38\u3001\u9ad8\u5ea6\u306a\u30ac\u30b9\u30af\u30ed\u30de\u30c8\u30b0\u30e9\u30d5\u30a3\u30fc\u8cea\u91cf\u5206\u6790(GC-MS)\u3092\u7528\u3044\u3066\u5206\u6790\u3055\u308c\u307e\u3059\u304c\u3001\u305d\u306e\u624b\u6cd5\u306b\u306f\u6642\u9593\u304c\u304b\u304b\u308a\u3001\u30b3\u30b9\u30c8\u304c\u9ad8\u3044\u3068\u3044\u3046\u554f\u984c\u304c\u3042\u308a\u307e\u3059\u3002<\/p>\n\n\n\n<p>\u73fe\u5728\u3001\u591a\u304f\u306e\u30e9\u30dc\u3067\u306f\u3001MCPD\u306e\u5206\u6790\u306b\u304a\u3044\u3066\u30015%\u30b8\u30d5\u30a7\u30cb\u30eb\u300195%\u30b8\u30e1\u30c1\u30eb\u30dd\u30ea\u30b7\u30ed\u30ad\u30b5\u30f3\u307e\u305f\u306f50%\u30b8\u30d5\u30a7\u30cb\u30eb\u300150%\u30b8\u30e1\u30c1\u30eb\u30dd\u30ea\u30b7\u30ed\u30ad\u30b5\u30f3\u56fa\u5b9a\u76f8\u3092\u6301\u306430 m x 0.25 mm\u5185\u5f84 x 0.25 \u03bcm\u306e\u30ad\u30e3\u30d4\u30e9\u30ea\u30fc\u30ab\u30e9\u30e0\u3092\u4f7f\u7528\u3057\u3066\u3044\u307e\u3059\u3002\u5f93\u6765\u306eGC-MS\u3067\u306f\u5206\u6790\u6642\u9593\u304c12\u5206\u4ee5\u4e0a\u3068\u9577\u304f\u3001\u7d50\u679c\u3068\u3057\u30661\u5206\u6790\u3042\u305f\u308a\u306b\u6d88\u8cbb\u3059\u308b\u30d8\u30ea\u30a6\u30e0\u306e\u4f7f\u7528\u3082\u591a\u304f\u3001\u30b5\u30f3\u30d7\u30eb\u5206\u6790\u30b3\u30b9\u30c8\u3092\u62bc\u3057\u4e0a\u3052\u308b\u8981\u56e0\u3068\u306a\u3063\u3066\u3044\u307e\u3057\u305f\u3002<br>\u5927\u91cf\u306e\u30b5\u30f3\u30d7\u30eb\u3092\u51e6\u7406\u3059\u308b\u5fc5\u8981\u304c\u3042\u308b\u3088\u3046\u306a\u30b1\u30fc\u30b9\u306b\u304a\u3044\u3066\u30d8\u30ea\u30a6\u30e0\u30b3\u30b9\u30c8\u3092\u7bc0\u7d04\u3059\u308b\u306b\u306f\u3001\u30b5\u30f3\u30d7\u30eb\u30b9\u30eb\u30fc\u30d7\u30c3\u30c8\u3092\u5411\u4e0a\u3055\u305b\u3001\u5206\u6790\u6642\u9593\u3092\u77ed\u7e2e\u3059\u308b\u3053\u3068\u304c\u5fc5\u8981\u3068\u306a\u308a\u307e\u3059\u3002\u3057\u304b\u3057\u306a\u304c\u3089\u3001MCPD\u5206\u6790\u306b\u304a\u3051\u308b\u5206\u6790\u6642\u9593\u306e\u77ed\u7e2e\u306f\u3001\u91cd\u8981\u306a\u7570\u6027\u4f53\u306e\u5206\u96e2\u60aa\u5316\u3092\u62db\u304f\u53ef\u80fd\u6027\u304c\u9ad8\u304f\u3001\u7d50\u679c\u3068\u3057\u3066\u30b9\u30eb\u30fc\u30d7\u30c3\u30c8\u3092\u6539\u5584\u3057\u306a\u304c\u3089\u3001\u5206\u96e2\u6027\u80fd\u3092\u7dad\u6301\u3059\u308b\u3053\u3068\u306f\u3001MCPD\u5206\u6790\u306b\u304a\u3044\u3066\u975e\u5e38\u306b\u96e3\u3057\u3044\u8ab2\u984c\u3068\u3057\u3066\u5b58\u5728\u3057\u3066\u3044\u307e\u3059\u3002<\/p>\n\n\n\n<p>\u305d\u3053\u3067\u6ce8\u76ee\u3055\u308c\u308b\u306e\u304c\u3001\u4f4e\u5727\u30ac\u30b9\u30af\u30ed\u30de\u30c8\u30b0\u30e9\u30d5\u30a3\u30fc\uff08LPGC\uff09\u3068\u3044\u3046\u6280\u8853\u3067\u3059\u3002\u3053\u306e\u6280\u8853\u306f\u3001\u30ab\u30e9\u30e0\u5185\u5727\u529b\u3092\u4f4e\u6e1b\u3059\u308b\u3053\u3068\u306b\u3088\u308a\u3001\u5206\u6790\u6642\u9593\u3068\u30d8\u30ea\u30a6\u30e0\u4f7f\u7528\u91cf\u3092\u524a\u6e1b\u3059\u308b\u3053\u3068\u304c\u53ef\u80fd\u3067\u3059\u3002\u5f53\u793e\u306eLPGC Rxi-17Sil MS \u30ad\u30c3\u30c8(cat.# 11805)\u3092\u4f7f\u7528\u3059\u308b\u3053\u3068\u3067\u3001\u5f93\u6765\u306e\u65b9\u6cd5\u306b\u6bd4\u3079\u3066\u5206\u6790\u6642\u9593\u304c1\/2\u306b\u77ed\u7e2e\u3001\u30d8\u30ea\u30a6\u30e0\u6d88\u8cbb\u306b\u3064\u3044\u3066\u306f69%\u3082\u524a\u6e1b\u3067\u304d\u308b\u3053\u3068\u304c\u5b9f\u969b\u306e\u5206\u6790\u306b\u304a\u3044\u3066\u793a\u3055\u308c\u3066\u3044\u307e\u3059\u3002\u3053\u308c\u306b\u3088\u308a\u3001\u30e9\u30dc\u306f\u3088\u308a\u591a\u304f\u306e\u30b5\u30f3\u30d7\u30eb\u3092\u3088\u308a\u52b9\u7387\u7684\u304b\u3064\u7d4c\u6e08\u7684\u306b\u5206\u6790\u3067\u304d\u308b\u3088\u3046\u306b\u306a\u308a\u307e\u3059\u3002<\/p>\n\n\n\n<p>\u3053\u306eLPGC\u6280\u8853\u306f\u30012-MCPD\u30843-MCPD\u3068\u3044\u3063\u305f\u91cd\u8981\u306a\u7570\u6027\u4f53\u306b\u5bfe\u3057\u3066\u512a\u308c\u305f\u5206\u96e2\u6027\u80fd\u3092\u6301\u3061\u3001\u8a98\u5c0e\u4f53\u5316\u8a66\u85ac\u6210\u5206\u3068\u3082\u5341\u5206\u306a\u5206\u96e2\u3092\u5b9f\u73fe\u3057\u307e\u3059\u3002\u307e\u305f\u3001\u30ab\u30e9\u30e0\u4ea4\u63db\u3082\u5bb9\u6613\u3067\u3001\u901a\u5e38\u306e\u30ad\u30e3\u30d4\u30e9\u30ea\u30fc\u30ab\u30e9\u30e0\u540c\u69d8\u306b\u7c21\u5358\u306b\u30e1\u30f3\u30c6\u30ca\u30f3\u30b9\u3084\u4ea4\u63db\u4f5c\u696d\u304c\u884c\u3048\u307e\u3059\u3002\u5404LPGC\u30ad\u30c3\u30c8\u306f\u3001\u30ea\u30fc\u30af\u304c\u306a\u3044\u3053\u3068\u3092\u4fdd\u8a3c\u3059\u308b\u305f\u3081\u306bRestek\u306e\u5de5\u5834\u3067\u500b\u5225\u306b\u691c\u67fb\u3055\u308c\u305f\u5f8c\u306b\u51fa\u8377\u3055\u308c\u3066\u304a\u308a\u3001Restek\u304c\u63b2\u3052\u308bPlus-One\u306e\u54c1\u8cea\u57fa\u6e96\u306b\u57fa\u3065\u3044\u3066\u3001\u304a\u5ba2\u69d8\u306b\u5b89\u5fc3\u3057\u3066\u3054\u4f7f\u7528\u3044\u305f\u3060\u3051\u308b\u88fd\u54c1\u3092\u63d0\u4f9b\u3057\u3066\u3044\u307e\u3059\u3002<\/p>\n\n\n\n<p>\u3053\u306e\u6280\u8853\u306e\u5c0e\u5165\u306b\u3088\u308a\u3001\u98df\u54c1\u5b89\u5168\u6027\u306e\u78ba\u4fdd\u3068\u30e9\u30dc\u306e\u904b\u55b6\u30b3\u30b9\u30c8\u306e\u524a\u6e1b\u3092\u540c\u6642\u306b\u9054\u6210\u3059\u308b\u3053\u3068\u304c\u53ef\u80fd\u3067\u3059\u3002\u98df\u54c1\u306e\u5b89\u5168\u3068\u54c1\u8cea\u3092\u5b88\u308b\u305f\u3081\u306b\u3082\u3001\u65b0\u3057\u3044\u5206\u6790\u6280\u8853\u306e\u5c0e\u5165\u3068\u305d\u306e\u6709\u52b9\u6d3b\u7528\u3092\u3054\u691c\u8a0e\u304f\u3060\u3055\u3044\u3002<br>\u00a0LPGC\u6280\u8853\u306e\u8a73\u7d30\u306b\u3064\u3044\u3066\u306f\u3053\u3061\u3089\u3092\u3054\u89a7\u304f\u3060\u3055\u3044\uff1a<a href=\"https:\/\/discover.restek.com\/ja\/articles-ja\/gnar3505-ja\/japanese-an-introduction-to-low-pressure-gc-ms-lpgc-ms\" data-type=\"link\" data-id=\"https:\/\/discover.restek.com\/ja\/articles-ja\/GNAR3505-JA\/japanese-an-introduction-to-low-pressure-gc-ms-lpgc-ms\">www.restek.com\/lpgc<\/a><\/p>\n\n\n<div class=\"wp-block-custom-chromatogram-article-top\"><div class=\"chromatogram-article-placeholder\"><div class=\"figure-heading\"><strong>Figure 1:\u00a0<\/strong>MCPD\u306b\u95a2\u3059\u308bLPGC Rxi-17Sil MS \u3068\u5f93\u6765\u306eGC-MS\u306e\u6bd4\u8f03\uff08\u30d4\u30fc\u30af\u30ea\u30b9\u30c8\u3068\u5206\u6790\u6761\u4ef6\u3092\u542b\u3080\u5b8c\u5168\u7248\u306fPDF\u3067\u30c0\u30a6\u30f3\u30ed\u30fc\u30c9\u53ef\uff09<\/div><div class='chromatogram-article-inner-full'><div class=\"chromatogram-article-inner\">\n<div class=\"wp-block-custom-chromatogram-article\"><div class=\"wp-block-custom-chromatogram-article\"><div class=\"chromatogram-image wide-image\"><img decoding=\"async\" src=\"https:\/\/ez.restek.com\/images\/cgram\/gc_fs0595.png\" alt=\"Comparison of Conventional and LPGC Analysis of 2-MCPD and 3-MCPD\" title=\"-\"><\/div><p class=\"article-id\" style=\"text-align:center\"> GC_FS0595<\/p><div class=\"chromatogram-pdf-link\"><a href=\"https:\/\/ez.restek.com\/images\/cgram\/gc_fs0595.pdf\" target=\"_blank\" rel=\"noopener noreferrer\"><svg xmlns=\"http:\/\/www.w3.org\/2000\/svg\" width=\"18\" height=\"18\" viewBox=\"0 0 18 18\"><g data-name=\"Group 2996\"><path data-name=\"Rectangle 1246\" d=\"M0 0h18v18H0z\" style=\"fill: none;\"><\/path><\/g><g data-name=\"Group 2997\"><path data-name=\"Path 729\" d=\"M13.412 11.4v2.017H5.345V11.4H4v2.017a1.349 1.349 0 0 0 1.345 1.345h8.068a1.349 1.349 0 0 0 1.345-1.345V11.4zm-.672-2.694-.948-.948-1.741 1.735V4H8.706v5.493L6.965 7.758l-.948.948 3.361 3.361z\" transform=\"translate(-.437 -.414)\" style=\"fill: rgb(13, 123, 196);\"><\/path><\/g><\/svg>Download PDF<\/a><\/div><\/div><\/div>\n<\/div><\/div><\/div>\n\n\n<div style=\"height:100px\" aria-hidden=\"true\" class=\"wp-block-spacer\"><\/div>\n\n\n        <div class=\"cpb\">\n            <h3 class=\"cpb-heading\">Products Mentioned<\/h3>\n            <hr class=\"cpb-heading-underline\" \/>\n            <div class=\"cpb-list\">\n                                    <div class=\"cpb-item\">\n                        <div class=\"cpb-col cpb-col--left\">\n                            <a class=\"cpb-catalog\" target=\"_blank\" rel=\"noopener noreferrer\" href=\"https:\/\/www.restek.com\/p\/11805\">                                Catalog No. 11805                            <\/a>                        <\/div>\n                        <div class=\"cpb-col cpb-col--middle\">\n                            <div class=\"cpb-title\">LPGC Rxi-17Sil MS\u30ab\u30e9\u30e0\u30ad\u30c3\u30c8<\/div>\n                        <\/div>\n                        <div class=\"cpb-col cpb-col--right\">\n                                                            <a class=\"cpb-view-btn\" target=\"_blank\" rel=\"noopener noreferrer\" href=\"https:\/\/www.restek.com\/p\/11805\">\u88fd\u54c1\u60c5\u5831\u3092\u898b\u308b<\/a>\n                                                    <\/div>\n                    <\/div>\n                                    <div class=\"cpb-item\">\n                        <div class=\"cpb-col cpb-col--left\">\n                            <a class=\"cpb-catalog\" target=\"_blank\" rel=\"noopener noreferrer\" href=\"https:\/\/www.restek.com\/p\/14123\">                                Catalog No. 14123                            <\/a>                        <\/div>\n                        <div class=\"cpb-col cpb-col--middle\">\n                            <div class=\"cpb-title\">Rxi-17Sil MS GC Capillary Column, 30 m, 0.25 mm ID, 0.25 \u00b5m<\/div>\n                        <\/div>\n                        <div class=\"cpb-col cpb-col--right\">\n                                                            <a class=\"cpb-view-btn\" target=\"_blank\" rel=\"noopener noreferrer\" href=\"https:\/\/www.restek.com\/p\/14123\">\u88fd\u54c1\u60c5\u5831\u3092\u898b\u308b<\/a>\n                                                    <\/div>\n                    <\/div>\n                                    <div class=\"cpb-item\">\n                        <div class=\"cpb-col cpb-col--left\">\n                            <a class=\"cpb-catalog\" target=\"_blank\" rel=\"noopener noreferrer\" href=\"https:\/\/www.restek.com\/p\/23303\">                                Catalog No. 23303                            <\/a>                        <\/div>\n                        <div class=\"cpb-col cpb-col--middle\">\n                            <div class=\"cpb-title\">Topaz, Single Taper Inlet Liner, 4.0 mm x 6.5 x 78.5, for Agilent GCs, w\/Quartz Wool, Premium Deactivation, 5-pk.<\/div>\n                        <\/div>\n                        <div class=\"cpb-col cpb-col--right\">\n                                                            <a class=\"cpb-view-btn\" target=\"_blank\" rel=\"noopener noreferrer\" href=\"https:\/\/www.restek.com\/p\/23303\">\u88fd\u54c1\u60c5\u5831\u3092\u898b\u308b<\/a>\n                                                    <\/div>\n                    <\/div>\n                                    <div class=\"cpb-item\">\n                        <div class=\"cpb-col cpb-col--left\">\n                            <a class=\"cpb-catalog\" target=\"_blank\" rel=\"noopener noreferrer\" href=\"https:\/\/www.restek.com\/p\/21143\">                                Catalog No. 21143                            <\/a>                        <\/div>\n                        <div class=\"cpb-col cpb-col--middle\">\n                            <div class=\"cpb-title\">Short-Cap Vial with Grad Marking Spot, 9-425 Screw-Thread, 2.0 mL, 9 mm, 12 x 32 (vial only), Amber, 1000-pk.<\/div>\n                        <\/div>\n                        <div class=\"cpb-col cpb-col--right\">\n                                                            <a class=\"cpb-view-btn\" target=\"_blank\" rel=\"noopener noreferrer\" href=\"https:\/\/www.restek.com\/p\/21143\">\u88fd\u54c1\u60c5\u5831\u3092\u898b\u308b<\/a>\n                                                    <\/div>\n                    <\/div>\n                                    <div class=\"cpb-item\">\n                        <div class=\"cpb-col cpb-col--left\">\n                            <a class=\"cpb-catalog\" target=\"_blank\" rel=\"noopener noreferrer\" href=\"https:\/\/www.restek.com\/p\/24495\">                                Catalog No. 24495                            <\/a>                        <\/div>\n                        <div class=\"cpb-col cpb-col--middle\">\n                            <div class=\"cpb-title\">Short Screw Caps, Polypropylene, Screw-Thread, PTFE\/Silicone\/PTFE Septa, Black, Preassembled, 2.0 mL, 9 mm, 100-pk.<\/div>\n                        <\/div>\n                        <div class=\"cpb-col cpb-col--right\">\n                                                            <a class=\"cpb-view-btn\" target=\"_blank\" rel=\"noopener noreferrer\" href=\"https:\/\/www.restek.com\/p\/24495\">\u88fd\u54c1\u60c5\u5831\u3092\u898b\u308b<\/a>\n                                                    <\/div>\n                    <\/div>\n                            <\/div>\n        <\/div>\n        \n\n\n<div style=\"height:100px\" aria-hidden=\"true\" class=\"wp-block-spacer\"><\/div>\n","protected":false},"excerpt":{"rendered":"<p>\u4f4e\u5727\u30ac\u30b9\u30af\u30ed\u30de\u30c8\u30b0\u30e9\u30d5\u30a3\u30fc\uff08LPGC\uff09\u306b\u3088\u308bMCPD\u306e\u8fc5\u901f\u5206\u6790\u306f\u5f93\u6765\u306eGC-MS\u5206\u6790\u3088\u308a\u30822\u500d\u901f\u304f\u3001\u30d8\u30ea\u30a6\u30e0\u6d88\u8cbb\u3082\u6700\u5927 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