{"id":48564,"date":"2023-04-03T14:30:00","date_gmt":"2023-04-03T14:30:00","guid":{"rendered":"https:\/\/discover.restek.com\/uncategorized\/pfas-epa-1633-and-bile-acids-japan\/"},"modified":"2026-02-18T17:53:44","modified_gmt":"2026-02-18T17:53:44","slug":"pfas-epa-1633-and-bile-acids-japan","status":"publish","type":"post","link":"https:\/\/discover.restek.com\/ja\/blogs-ja\/gnbl4765-ja\/pfas-epa-1633-and-bile-acids-japan","title":{"rendered":"\u7c73\u56fdEPA 1633\u306b\u3088\u308bPFAS\u5206\u6790: \u30a2\u30bb\u30c8\u30cb\u30c8\u30ea\u30eb\u306e\u4f7f\u7528\u3067\u80c6\u6c41\u9178\u5206\u96e2\u3092\u6700\u9069\u5316"},"content":{"rendered":"\n

\u3053\u306e\u8a18\u4e8b\u306b\u30a2\u30af\u30bb\u30b9\u3057\u305f\u3068\u3044\u3046\u3053\u3068\u306f\u3001EPA\u304c\u767a\u884c\u3057\u305f\u8349\u6848\u300cAnalysis of Per- and Polyfluoroalkyl Substances (PFAS) in Aqueous, Solid, Biosolids, and Tissue Samples by LC-MS\/MS<\/a>.\u300d\u306b\u6df1\u3044\u95a2\u5fc3\u3092\u304a\u6301\u3061\u3067\u3042\u308b\u3053\u3068\u3068\u601d\u3044\u307e\u3059\u3002\u8349\u6848\u306b\u306f\u300141\u7a2e\u985e\u306ePFAS\u5316\u5408\u7269\u3092\u5206\u6790\u3059\u308b\u969b\u306e\u91cd\u8981\u306a\u30ac\u30a4\u30c9\u30e9\u30a4\u30f3\u304c\u8a18\u8f09\u3055\u308c\u3066\u3044\u307e\u3059\u3002\u305d\u306e\u4e2d\u3067\u3082\u7279\u306b\u6ce8\u76ee\u3059\u3079\u304d\u306f\u3001\u80c6\u6c41\u9178\u3068PFOS\uff08\u30d1\u30fc\u30d5\u30eb\u30aa\u30ed\u30aa\u30af\u30bf\u30f3\u30b9\u30eb\u30db\u30f3\u9178\uff09\u306e\u5e72\u6e09\u306b\u3064\u3044\u3066\u3067\u3059\u3002PFAS\u306e\u5206\u6790\u65b9\u6cd5\u306b\u304a\u3044\u3066\u3001\u80c6\u6c41\u9178\u304c\u3069\u306e\u3088\u3046\u306bPFOS\u306b\u5e72\u6e09\u3059\u308b\u304b\u306f\u3001\u4f7f\u7528\u3055\u308c\u308b\u79fb\u52d5\u76f8\u306e\u6709\u6a5f\u6eb6\u5a92\u306b\u3088\u3063\u3066\u5927\u304d\u304f\u7570\u306a\u308b\u3053\u3068\u304c\u793a\u3055\u308c\u3066\u3044\u307e\u3059\u3002\u4f8b\u3048\u3070\u3001\u30a2\u30bb\u30c8\u30cb\u30c8\u30ea\u30eb\u3092\u4f7f\u7528\u3057\u305f\u5834\u5408\u3001\u80c6\u6c41\u9178\u306e\u4e00\u7a2e\u3067\u3042\u308b\u30bf\u30a6\u30ed\u30c7\u30aa\u30ad\u30b7\u30b3\u30fc\u30eb\u9178\uff08TDCA\uff09\u3092\u30e2\u30cb\u30bf\u30ea\u30f3\u30b0\u3059\u308b\u5fc5\u8981\u304c\u3042\u308a\u307e\u3059\u3002\u305d\u3057\u3066\u3001\u3053\u306e\u80c6\u6c41\u9178\u3068PFOS\u306f\u3001\u5c11\u306a\u304f\u3068\u30821\u5206\u4ee5\u4e0a\u306e\u9593\u9694\u3092\u7a7a\u3051\u3066\u5206\u96e2\u3059\u308b\u3053\u3068\u304c\u63a8\u5968\u3055\u308c\u3066\u3044\u307e\u3059\u3002\u307e\u305f\u3001\u30e1\u30bf\u30ce\u30fc\u30eb\u306a\u3069\u4ed6\u306e\u6709\u6a5f\u6eb6\u5a92 \u3092\u4f7f\u7528\u3059\u308b\u5834\u5408\u306b\u306f\u3001\u30bf\u30a6\u30ed\u30d8\u30ce\u30c7\u30aa\u30ad\u30b7\u30b3\u30fc\u30eb\u9178\uff08TCDCA\uff09\u3084\u30bf\u30a6\u30ed\u30a6\u30eb\u30bd\u30c7\u30aa\u30ad\u30b7\u30b3\u30fc\u30eb\u9178\uff08TUDCA\uff09\u3092\u542b\u3081\u305f3\u3064\u306e\u80c6\u6c41\u9178\u304c\u3001PFOS\u3068\u306e\u9593\u30671\u5206\u4ee5\u4e0a\u306e\u4fdd\u6301\u6642\u9593\u3092\u78ba\u4fdd\u3059\u308b\u5fc5\u8981\u304c\u3042\u308b\u3053\u3068\u3082\u8a18\u8f09\u3055\u308c\u3066\u3044\u307e\u3059\u3002\u3053\u306e\u4fdd\u6301\u6642\u9593\u306e\u78ba\u4fdd\u306f\u3001\u9ad8\u7cbe\u5ea6\u306a\u5206\u6790\u3092\u5b9f\u73fe\u3059\u308b\u305f\u3081\u306b\u306f\u6b20\u304b\u305b\u307e\u305b\u3093\u3002\u3055\u3089\u306b\u3001\u4fdd\u6301\u6642\u9593\u306e\u8981\u4ef6\u306b\u52a0\u3048\u3066\u3001\u80c6\u6c41\u9178\u306f\u3044\u304b\u306a\u308bPFAS\u5206\u6790\u5bfe\u8c61\u6210\u5206\u3068\u5171\u6eb6\u51fa\u3057\u306a\u3044\u3053\u3068\u3082\u91cd\u8981\u3067\u3059\u3002\u3053\u308c\u306b\u3088\u308a\u3001\u5206\u6790\u306e\u7cbe\u5ea6\u304c\u78ba\u4fdd\u3055\u308c\u3001\u6b63\u78ba\u306a\u7d50\u679c\u304c\u5f97\u3089\u308c\u307e\u3059\u3002\u30a2\u30bb\u30c8\u30cb\u30c8\u30ea\u30eb\u3092\u4f7f\u7528\u3057\u3066\u3001\u3053\u306e\u3088\u3046\u306a\u30ac\u30a4\u30c9\u30e9\u30a4\u30f3\u3092\u6e80\u305f\u3059\u65b9\u6cd5\u3092\u78ba\u7acb\u3057\u305f\u306e\u3067\u3001\u6700\u9069\u5316\u3055\u308c\u305f\u6761\u4ef6\u3067PFAS\u306e\u5206\u6790\u304c\u884c\u3048\u308b\u3088\u3046\u306b\u306a\u3063\u3066\u3044\u307e\u3059\u3002<\/p>\n\n\n

\u30a2\u30bb\u30c8\u30cb\u30c8\u30ea\u30eb\u3092\u4f7f\u7528\u3057\u305fLC-MS\/MS\u306b\u3088\u308bForce C18\u30ab\u30e9\u30e0\u3067\u306eEPA 1633 PFAS\u5206\u6790<\/strong>\uff08\u30d4\u30fc\u30af\u30ea\u30b9\u30c8\u3068\u5206\u6790\u6761\u4ef6\u3092\u542b\u3080\u5b8c\u5168\u7248\u306fPDF\u3067\u30c0\u30a6\u30f3\u30ed\u30fc\u30c9\u53ef\uff09<\/div>
\n
\"EPA<\/div>

LC_EV0585<\/p>

<\/path><\/g><\/path><\/g><\/svg>Download PDF<\/a><\/div><\/div><\/div>\n<\/div><\/div><\/div>\n\n\n
<\/div>\n\n\n\n

5mM\u9162\u9178\u30a2\u30f3\u30e2\u30cb\u30a6\u30e0\u3092\u542b\u3080\u6c34\u3068\u30a2\u30bb\u30c8\u30cb\u30c8\u30ea\u30eb\u3092\u79fb\u52d5\u76f8\u3068\u3057\u3066\u4f7f\u7528\u3057\u3001Force C18\u30ab\u30e9\u30e0<\/a>\u3092\u63a1\u7528\u3057\u305f\u3053\u306e\u30e1\u30bd\u30c3\u30c9\u306f\u3001\u975e\u5e38\u306b\u52b9\u7387\u7684\u306bPFOS\u3068\u80c6\u6c41\u9178\uff08TDCA\u306a\u3069\uff09\u3092\u5206\u96e2\u3057\u307e\u3059\u3002\u7d50\u679c\u3068\u3057\u3066\u3001PFOS\u306e\u4fdd\u6301\u6642\u9593\uff088.8\u5206\uff09\u306f\u3001TDCA\u306e\u4fdd\u6301\u6642\u9593\uff085.8\u5206\uff09\u304b\u30891\u5206\u4ee5\u4e0a\u5206\u96e2\u3055\u308c\u3001\u30b5\u30a4\u30af\u30eb\u30bf\u30a4\u30e0\u304c14\u5206\u3068\u3044\u3046\u975e\u5e38\u306b\u77ed\u3044\u6642\u9593\u3067\u5168PFAS\u6210\u5206\u3068TDCA\u306e\u5206\u96e2\u304c\u53ef\u80fd\u3068\u306a\u3063\u3066\u3044\u307e\u3059\u3002\u30a2\u30bb\u30c8\u30cb\u30c8\u30ea\u30eb\u3092\u4f7f\u7528\u3059\u308b\u3053\u3068\u306b\u3088\u308a\u30013\u3064\u306e\u80c6\u6c41\u9178\uff08TDCA\u3001TCDCA\u3001TUDCA\uff09\u3092PFOS\u3068\u306e\u5206\u96e2\u306b\u304a\u3044\u30661\u5206\u4ee5\u4e0a\u306e\u5206\u96e2\u3092\u78ba\u4fdd\u3059\u308b\u3053\u3068\u304c\u3067\u304d\u3001\u975e\u5e38\u306b\u52b9\u7387\u7684\u306a\u89e3\u6790\u304c\u53ef\u80fd\u3067\u3059\u3002\u305f\u3060\u3057\u3001TUDCA\uff08\u4fdd\u6301\u6642\u9593 = 5.5\u5206\uff09\u3068ADONA\uff08\u4fdd\u6301\u6642\u9593 = 5.7\u5206\uff09\u3068\u306e\u9593\u306b\u306f\u5341\u5206\u306a\u5206\u96e2\u304c\u5f97\u3089\u308c\u307e\u305b\u3093\u3067\u3057\u305f\u3002<\/p>\n\n\n\n

\"\"<\/figure>\n\n\n\n

\u79fb\u52d5\u76f8\u3092\u30e1\u30bf\u30ce\u30fc\u30eb\u306b\u5207\u308a\u66ff\u3048\u308b\u3068\u3069\u3046\u306a\u308b\u3067\u3057\u3087\u3046\u304b\uff1f\u30a2\u30bb\u30c8\u30cb\u30c8\u30ea\u30eb\u306e\u5834\u5408\u306b\u306f\u3001\u30e2\u30cb\u30bf\u30ea\u30f3\u30b0\u304c\u5fc5\u8981\u306a\u306e\u306f1\u3064\u306e\u80c6\u6c41\u9178\u5e72\u6e09\u306e\u307f\u3067\u3057\u305f\u3002\u3057\u304b\u3057\u3001\u30e1\u30bf\u30ce\u30fc\u30eb\u306e\u5834\u5408\u30013\u3064\u306e\u80c6\u6c41\u9178\u306b\u3064\u3044\u3066\u3001EPA 1633\u306e\u8981\u4ef6\u306b\u5f93\u3063\u3066\u4ed6\u306ePFAS\u5316\u5408\u7269\u3068\u5171\u6eb6\u51fa\u3057\u306a\u3044\u3053\u3068\u3068\u540c\u6642\u306b\u3001PFOS\u304b\u3089\u5c11\u306a\u304f\u3068\u30821\u5206\u306f\u5206\u96e2\u3055\u305b\u308b\u3053\u3068\u304c\u5fc5\u8981\u3067\u3059\u3002EPA 1633\u306e\u8981\u4ef6\u3092\u6e80\u305f\u3059\u5fc5\u8981\u304c\u3042\u308b\u3053\u3068\u306b\u52a0\u3048\u3066\u3001\u88c5\u7f6e\u306e\u4f7f\u7528\u52b9\u7387\u3092\u6700\u5927\u5316\u3057\u305f\u3044\u305f\u3081\u3001\u53ef\u80fd\u306a\u9650\u308a\u30b5\u30a4\u30af\u30eb\u30bf\u30a4\u30e0\u3092\u77ed\u7e2e\u3059\u308b\u3053\u3068\u3082\u91cd\u8981\u3067\u3059\u3002\u79fb\u52d5\u76f8\u306b\u30e1\u30bf\u30ce\u30fc\u30eb\u3092\u4f7f\u7528\u3057\u305f\u30e1\u30bd\u30c3\u30c9\u30b9\u30ab\u30a6\u30c6\u30a3\u30f3\u30b0\u30af\u30ed\u30de\u30c8\u30b0\u30e9\u30e0\uff08\u30b9\u30af\u30ea\u30fc\u30cb\u30f3\u30b0\u5b9f\u9a13\uff09\u3092\u898b\u3066\u307f\u307e\u3057\u3087\u3046\u3002<\/p>\n\n\n\n

\u30ab\u30e9\u30e0:<\/td>Raptor C18 with Guard <\/td><\/tr>
\u5bf8\u6cd5:<\/td>50 mm x 2.1 mm ID<\/td><\/tr>
\u7c92\u5b50\u30b5\u30a4\u30ba:<\/td>1.8 \u00b5m<\/td><\/tr>
\u6e29\u5ea6:<\/td>30 \u00b0C<\/td><\/tr>
\u6a19\u6e96\u8a66\u6599\/\u30b5\u30f3\u30d7\u30eb:<\/td>PFAS 1633<\/td><\/tr>
\u5e0c\u91c8\u5264:<\/td>\u6c34<\/td><\/tr>
\u6ce8\u5165\u91cf:<\/td>1 \u00b5L<\/td><\/tr>
\u79fb\u52d5\u76f8A:<\/td>5 mM\u9162\u9178\u30a2\u30f3\u30e2\u30cb\u30a6\u30e0\u6c34\u6eb6\u6db2<\/td><\/tr>
\u79fb\u52d5\u76f8B:<\/td>\u30e1\u30bf\u30ce\u30fc\u30eb<\/td><\/tr>
\u6ce8\u5165\u91cf:<\/td>10 \u00b5L<\/td><\/tr><\/tbody><\/table><\/figure>\n\n\n\n

\u6d41\u901f\uff1a0.4 mL\/min\u3000<\/p>\n\n\n\n

\u30b0\u30e9\u30b8\u30a8\u30f3\u30c8\uff1a40% B (0\u5206) \u2192 75% B (10.00\u5206)  \u2192 100% B (12.00\u5206)  \u2192 100% B (13.00\u5206)  \u2192  40% B (13.01\u5206)  \u2192  40% B (15.00\u5206)<\/p>\n\n\n\n

\"\"<\/figure>\n\n\n\n

\u30b9\u30ab\u30a6\u30c6\u30a3\u30f3\u30b0\u30b0\u30e9\u30b8\u30a8\u30f3\u30c8\u3092\u4f7f\u7528\u3057\u3066\u3001EPA 1633\u6a19\u6e96\u8a66\u6599\u3068\u80c6\u6c41\u9178\u306e\u6df7\u5408\u7269\u3092\u5206\u6790\u3057\u3001\u305d\u308c\u305e\u308c\u306e\u4fdd\u6301\u6642\u9593\u3092\u6bd4\u8f03\u3057\u307e\u3057\u305f\u3002\u30e1\u30bf\u30ce\u30fc\u30eb\u3092\u4f7f\u7528\u3057\u305f\u5834\u5408\u3001EPA 1633\u306e\u8981\u4ef6\u3092\u6e80\u305f\u3059\u5206\u96e2\u306f\u5341\u5206\u306b\u9054\u6210\u3067\u304d\u307e\u305b\u3093\u3067\u3057\u305f\u3002\u30e1\u30bf\u30ce\u30fc\u30eb\u306b\u3088\u308b\u30a2\u30d7\u30ed\u30fc\u30c1\u3067\u306f\u3001PFOS\u3068\u6700\u3082\u6eb6\u51fa\u6642\u9593\u306e\u8fd1\u3044\u80c6\u6c41\u9178\uff08TCDCA\uff09\u3068\u306e\u5206\u96e2\u306f\u308f\u305a\u304b0.263\u5206\u3067\u3057\u305f\u3002\u6b21\u306b\u3001\u5206\u6790\u6642\u9593\u3092\u9577\u304f\u3057\u300140\uff5e75\uff05\u306e\u30b0\u30e9\u30b8\u30a8\u30f3\u30c9\u6642\u9593\u30922\u5206\u8ffd\u52a0\u3057\u3001\u3053\u306e\u30e1\u30bd\u30c3\u30c9\u3092\u518d\u5ea6\u30c6\u30b9\u30c8\u3057\u307e\u3057\u305f\u3002<\/p>\n\n\n\n

\"\"<\/figure>\n\n\n\n

\u3053\u306e\u8abf\u6574\u3067\u3001PFOS\u3068\u6700\u3082\u6eb6\u51fa\u6642\u9593\u306e\u8fd1\u3044\u80c6\u6c41\u9178\u3067\u3042\u308bTCDCA\u3068\u306e\u5206\u96e2\u306f\u308f\u305a\u304b\u306b\u6539\u5584\u3057\u307e\u3057\u305f\u304c\u3001\u305d\u306e\u4ee3\u511f\u3068\u3057\u3066\u30e1\u30bd\u30c3\u30c9\u306e\u30b5\u30a4\u30af\u30eb\u30bf\u30a4\u30e0\u304c\u9577\u304f\u306a\u308a\u3001\u7406\u60f3\u7684\u306a\u5206\u6790\u6642\u9593\u3092\u78ba\u4fdd\u3059\u308b\u3053\u3068\u304c\u96e3\u3057\u3044\u3068\u3044\u3046\u7d50\u679c\u304c\u5f97\u3089\u308c\u307e\u3057\u305f\u3002\u3057\u305f\u304c\u3063\u3066\u3001EPA 1633\u306e\u8981\u4ef6\u3092\u5341\u5206\u306b\u6e80\u305f\u3059\u305f\u3081\u306b\u306f\u3001\u30a2\u30bb\u30c8\u30cb\u30c8\u30ea\u30eb\u304c\u6700\u9069\u306a\u79fb\u52d5\u76f8\u306e\u6709\u6a5f\u6eb6\u5a92\u3067\u3042\u308b\u3053\u3068\u304c\u5206\u304b\u308a\u307e\u3059\u3002\u540c\u6642\u306b\u77ed\u3044\u30b5\u30a4\u30af\u30eb\u30bf\u30a4\u30e0\u3067\u52b9\u7387\u7684\u306a\u5206\u6790\u304c\u53ef\u80fd\u3067\u3042\u308b\u3053\u3068\u3082\u8a3c\u660e\u3055\u308c\u307e\u3057\u305f\u3002<\/p>\n\n\n\n

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