{"id":71868,"date":"2025-11-26T21:16:00","date_gmt":"2025-11-26T21:16:00","guid":{"rendered":"https:\/\/discover.restek.com\/?p=71868"},"modified":"2026-03-03T04:58:29","modified_gmt":"2026-03-03T04:58:29","slug":"strengthened-pfos-and-pfoa-regulations-prepare-for-the-water-supply-act-revision-now-resteks-complete-guide-to-pfas-analysis-part-5-ja","status":"publish","type":"post","link":"https:\/\/discover.restek.com\/ja\/articles-ja\/jpsa2025-05\/strengthened-pfos-and-pfoa-regulations-prepare-for-the-water-supply-act-revision-now-resteks-complete-guide-to-pfas-analysis-part-5-ja","title":{"rendered":"PFOS\u30fbPFOA\u898f\u5236\u5f37\u5316\u5bfe\u7b56\uff5c\u4eca\u3053\u305d\u5099\u3048\u308b\uff01\u6c34\u9053\u6cd5\u6539\u6b63\u5bfe\u5fdc PFAS\u5206\u6790\u5b8c\u5168\u30ac\u30a4\u30c95"},"content":{"rendered":"\n

\uff1c\u30b7\u30ea\u30fc\u30ba\u8a73\u7d30\uff1e<\/strong>
\u7b2c1\u56de\uff1a<\/strong>\u6c34\u9053\u6cd5\u6539\u6b63\u306e\u80cc\u666f\u3068\u6982\u8981<\/a><\/strong>
\u7b2c2\u56de\uff1a\u5236\u5ea6\u6539\u6b63\u306e\u80cc\u666f\u3068PFOS\u30fbPFOA\u306e\u767a\u751f\u6e90\u30ea\u30b9\u30af\u3092\u6b63\u3057\u304f\u7406\u89e3\u3059\u308b<\/a>
\u7b2c3\u56de\uff1aPFOS\u30fbPFOA\u304c\u4e0e\u3048\u308b\u5065\u5eb7\u30fb\u74b0\u5883\u5f71\u97ff\u3068\u6c34\u8cea\u57fa\u6e96\u306e\u79d1\u5b66\u7684\u6839\u62e0<\/a>
\u7b2c4\u56de\uff1aPFAS\u5206\u6790\u306b\u6c42\u3081\u3089\u308c\u308b\u6280\u8853\u57fa\u6e96\u3068\u7559\u610f\u70b9<\/a>
\u7b2c5\u56de\uff1aPFAS\u5206\u6790\u3092\u652f\u3048\u308bRestek\u88fd\u54c1\u3068\u6700\u65b0\u30e1\u30bd\u30c3\u30c9\u306e\u5c0e\u5165\u4e8b\u4f8b<\/strong><\/p>\n\n\n\n

\u25a0 Restek \u304c\u3067\u304d\u308b\u3053\u3068\uff1aPFOS\u30fbPFOA \u5206\u6790\u5bfe\u5fdc\u30bd\u30ea\u30e5\u30fc\u30b7\u30e7\u30f3<\/h2>\n\n\n\n

PFOS\u30fbPFOA\u309250 ng\/L\u30ec\u30d9\u30eb\u3068\u3044\u3046\u6975\u3081\u3066\u4f4e\u6fc3\u5ea6\u3067\u5b9a\u91cf\u3059\u308b\u306b\u306f\u3001\u30b5\u30f3\u30d7\u30eb\u524d\u51e6\u7406\u3001\u5206\u96e2\u7cbe\u5ea6\u3001\u30af\u30ed\u30de\u30c8\u30b0\u30e9\u30d5\u30a3\u30fc\u6027\u80fd\u3001\u6a19\u6e96\u7269\u8cea\u306e\u9078\u5b9a\u306a\u3069\u3001\u5168\u5de5\u7a0b\u306b\u308f\u305f\u308b\u54c1\u8cea\u78ba\u4fdd\u304c\u5fc5\u8981\u3067\u3059\u3002
Restek\u3067\u306f\u3001\u3053\u3046\u3057\u305f\u8981\u4ef6\u306b\u5bfe\u5fdc\u3059\u308b\u305f\u3081\u3001PFAS\u5206\u6790\u306b\u7279\u5316\u3057\u305f\u30b5\u30f3\u30d7\u30eb\u524d\u51e6\u7406\u88fd\u54c1\u3001\u30ab\u30e9\u30e0\uff08\u5206\u6790\uff0f\u30c7\u30a3\u30ec\u30a4\uff09\u3001\u6a19\u6e96\u7269\u8cea\u3092\u5e45\u5e83\u304f\u3054\u63d0\u4f9b\u3057\u3066\u3044\u307e\u3059\u3002\u7279\u306b\u3001\u7c73\u56fdEPA Method 533\u3001EPA Method 537\u3084EPA Method 1633\u306b\u6e96\u62e0\u3057\u305f\u30e1\u30bd\u30c3\u30c9\u5bfe\u5fdc\u88fd\u54c1\u3092\u591a\u6570\u53d6\u308a\u63c3\u3048\u3001\u65e5\u672c\u306e\u4eca\u5f8c\u306e\u5236\u5ea6\u8981\u4ef6\u306b\u3082\u6574\u5408\u6027\u3092\u6301\u3064\u5f62\u3067\u6d3b\u7528\u3044\u305f\u3060\u3051\u307e\u3059\u3002<\/p>\n\n\n\n

 1.  \u9ad8\u56de\u53ce\u7387\u30fb\u4f4e\u30d6\u30e9\u30f3\u30af\u306e\u524d\u51e6\u7406\u30ab\u30fc\u30c8\u30ea\u30c3\u30b8\uff1aPFAS\u5206\u6790\u7528 Resprep WAX\u30dd\u30ea\u30de\u30fcSPE\u30ab\u30fc\u30c8\u30ea\u30c3\u30b8<\/h2>\n\n\n\n

\u6c34\u9053\u6c34\u4e2d\u306ePFAS\u5206\u6790\u306b\u304a\u3044\u3066\u3001\u56fa\u76f8\u62bd\u51fa\uff08SPE\uff09\u306b\u3088\u308b\u6fc3\u7e2e\u3068\u7cbe\u88fd\u306f\u6700\u3082\u91cd\u8981\u306a\u524d\u51e6\u7406\u5de5\u7a0b\u3067\u3059\u3002\u4ee5\u4e0b\u306e\u88fd\u54c1\u304c\u6700\u9069\u3067\u3059\u3002
PFAS\u6c34\u9053\u6c34\u5206\u6790 \uff5cResprep WAX\u30dd\u30ea\u30de\u30fcSPE \u30ab\u30fc\u30c8\u30ea\u30c3\u30b8, 30 \u00b5m, 6 mL\/500 mg, 30 \u03bcm, 30-pk.<\/a>\uff08cat. # 28268\uff09<\/p>\n\n\n\n

\u7279\u9577<\/strong><\/th>\u5185\u5bb9<\/strong><\/th><\/tr><\/thead>
\u6c34\u9053\u6c34\u30fb\u98f2\u6599\u6c34\u4e2dPFAS\u306e\u524d\u51e6\u7406\u306b\u6700\u9069<\/td>\u9ad8\u3044\u56de\u53ce\u7387\u3068\u518d\u73fe\u6027\uff08RSD\uff09\u3092\u5b9f\u73fe\u3002\u8d85\u9ad8\u7d14\u5ea6\u30dd\u30ea\u30de\u30fc\u5145\u586b\u5264\u3092\u4f7f\u3044\u3001\u5168\u30ed\u30c3\u30c8\u3067PFAS\u6c5a\u67d3\u691c\u67fb\u3092\u5b9f\u65bd\u3057\u6210\u7e3e\u8a66\u9a13\u66f8\uff08CoA\uff09\u3092\u6dfb\u4ed8\u3057\u3066\u4fe1\u983c\u6027\u3092\u4fdd\u8a3c<\/td><\/tr>
\u9006\u76f8\uff0b\u5f31\u9670\u30a4\u30aa\u30f3\u4ea4\u63db\u306e\u30df\u30c3\u30af\u30b9\u30e2\u30fc\u30c9<\/td>PFAS\u306e\u4fdd\u6301\u30fb\u6d17\u6d44\u30fb\u6eb6\u51fa\u3092\u52b9\u7387\u5316\u3002Restek\u72ec\u81ea\u306eDelay\u30ab\u30e9\u30e0\u3068\u306e\u4f75\u7528\u3067\u88c5\u7f6e\u7531\u6765\u306ePFAS\u30d0\u30c3\u30b0\u30b0\u30e9\u30a6\u30f3\u30c9\u3092\u4f4e\u6e1b\u3057\u3001\u5206\u6790\u306e\u30d0\u30c3\u30af\u30b0\u30e9\u30a6\u30f3\u30c9\u5bfe\u7b56\u3092\u5f37\u5316<\/td><\/tr>
pH 0\uff5e14\u306e\u5e83\u3044\u5b89\u5b9a\u6027\u3068\u9ad8\u6e7f\u6f64\u6027<\/td>\u52b9\u7387\u7684\u306a\u524d\u51e6\u7406\u3068\u6d41\u91cf\u4f9d\u5b58\u6027\u306e\u4f4e\u3055\u3067\u591a\u691c\u4f53\u51e6\u7406\u3084\u81ea\u52d5\u5316\u306b\u3082\u5bfe\u5fdc\u3002\u30cf\u30a4\u30b9\u30eb\u30fc\u30d7\u30c3\u30c8\u88c5\u7f6e\u904b\u7528\u3078\u306e\u62e1\u5f35\u53ef\u80fd<\/td><\/tr><\/tbody><\/table><\/figure>\n\n\n
Figure 8:<\/strong> \u6c34\u9053\u6c34\u6c34\u8cea\u691c\u67fb\u306b\u304a\u3044\u3066\u56fa\u76f8\u62bd\u51fa\u304c\u679c\u305f\u3059\u5f79\u5272<\/strong><\/div>
\n\n
\"\"<\/figure>\n\n<\/div><\/div><\/div>\n\n\n
<\/div>\n\n\n\n


\u307e\u305f\u3001\u74b0\u5883\u6c34\u30fb\u6392\u6c34\u306e\u5206\u6790\u306b\u306f\u4ee5\u4e0b\u306e\u88fd\u54c1\u3092\u4f7f\u7528\u3059\u308b\u306e\u304c\u6700\u9069\u3067\u3059\u3002
 PFAS\u5206\u6790\u7528 \u56fa\u76f8\u62bd\u51fa Resprep PFAS \u30ab\u30fc\u30c8\u30ea\u30c3\u30b8 | \u30d5\u30a3\u30eb\u30bf\u30fc\u30a8\u30a4\u30c9\u5165\u308a, 6 mL, Filter Aid 2000 mg\/WAX 150 mg\/GCB 50 mg, 30-pk.<\/a>\uff08cat. # 28931\uff09<\/p>\n\n\n\n

\u7279\u9577<\/strong><\/th>\u5185\u5bb9<\/strong><\/th><\/tr><\/thead>
PA 1633\u6e96\u62e0\u306e\u9ad8\u7d14\u5ea6WAX\u5145\u586b\u5264\u3068CarboPrep Plus GCB\u306e\u30c7\u30e5\u30a2\u30eb\u30d9\u30c3\u30c9\u69cb\u9020<\/td> PFAS\u306e\u5e83\u7bc4\u56f2\u306a\u5316\u5408\u7269\u3092\u9ad8\u56de\u53ce\u7387\u3067\u52b9\u7387\u7684\u306b\u6355\u6349\u3000PFAS\u6c5a\u67d3\u691c\u67fb\u6e08\u307f\u3067\u5fae\u91cf\u6e2c\u5b9a\u306e\u4fe1\u983c\u6027\u3092\u78ba\u4fdd<\/td><\/tr>
\u30d5\u30a3\u30eb\u30bf\u30fc\u30a8\u30a4\u30c9\u63a1\u7528<\/td>\u30b5\u30f3\u30d7\u30eb\u4e2d\u306e\u7c92\u5b50\u76ee\u8a70\u307e\u308a\u3092\u9632\u6b62\u3057\u3001\u30ac\u30e9\u30b9\u30a6\u30fc\u30eb\u5145\u586b\u3088\u308a\u3082\u77ed\u6642\u9593\u304b\u3064\u5b89\u5b9a\u3057\u305f\u901a\u6c34\u304c\u53ef\u80fd\u3000\u624b\u4f5c\u696d\u306e\u308d\u904e\u3092\u7701\u304d\u3001\u524d\u51e6\u7406\u306e\u4f5c\u696d\u52b9\u7387\u3068\u518d\u73fe\u6027\u3092\u5411\u4e0a<\/td><\/tr>
\u771f\u7a7a\u30de\u30cb\u30db\u30fc\u30eb\u30c9\u3084\u81ea\u52d5\u5316\u30b7\u30b9\u30c6\u30e0\u306b\u5bfe\u5fdc\u53ef\u80fd\u306a\u5e45\u5e83\u3044\u4e92\u63db\u6027<\/td>\u975e\u98f2\u6599\u6c34\u3001\u571f\u58cc\u3001\u30d0\u30a4\u30aa\u30bd\u30ea\u30c3\u30c9\u3001\u7d44\u7e54\u306a\u3069\u8907\u96d1\u30de\u30c8\u30ea\u30c3\u30af\u30b9\u306e\u30eb\u30fc\u30c1\u30f3\u5206\u6790\u306b\u6700\u9069\u306a\u524d\u51e6\u7406\u30ef\u30fc\u30af\u30d5\u30ed\u30fc\u3092\u63d0\u4f9b<\/td><\/tr><\/tbody><\/table><\/figure>\n\n\n\n

\u3053\u306e\u8a18\u4e8b\u300cPFAS SPE \u30b5\u30f3\u30d7\u30eb\u524d\u51e6\u7406\u3000Resprep\u7a4d\u5c64\u56fa\u76f8\u30ab\u30fc\u30c8\u30ea\u30c3\u30b8\u3067\u52b9\u7387\u7684\u306a\u62bd\u51fa\u3068\u30af\u30ea\u30fc\u30f3\u30a2\u30c3\u30d7\u3092\u5b9f\u73fe\uff01<\/a>\u300d\u304b\u3089\u3001\u8a73\u7d30\u306a\u60c5\u5831\u3092\u3054\u78ba\u8a8d\u4e0b\u3055\u3044\uff01<\/p>\n\n\n

Figure 9\uff1a\u7a4d\u5c64\u56fa\u76f8\u30ab\u30fc\u30c8\u30ea\u30c3\u30b8\u306e\u69cb\u6210<\/strong><\/div>
\n\n
\"\"<\/figure>\n\n<\/div><\/div><\/div>\n\n\n
<\/div>\n\n\n\n

2. PFAS\u5206\u6790\u306b\u9069\u3057\u305f\u30ab\u30e9\u30e04\u9078<\/h2>\n\n\n\n

PFAS\u5206\u6790\u306b\u304a\u3044\u3066\u30ab\u30e9\u30e0\u306b\u6c42\u3081\u3089\u308c\u3066\u3044\u308b\u306e\u306f\u3001\u9ad8\u611f\u5ea6\u306a\u4fdd\u6301\u3092\u5b9f\u73fe\u3057\u306a\u304c\u3089\u3082\u3001\u5206\u6790\u6642\u9593\u3092\u77ed\u7e2e\u3001\u30b9\u30eb\u30fc\u30d7\u30c3\u30c8\u3092\u5411\u4e0a\u3055\u305b\u308b\u3053\u3068\u3067\u3059\u3002\u307e\u305f\u3001\u8fd1\u5e74\u3067\u306f\u77ed\u9396\u30fb\u4e2d\u9396\u30fb\u9577\u9396\u306e\u6df7\u5728\u306b\u5bfe\u5fdc\u3067\u304d\u308b\u30ab\u30e9\u30e0\u306e\u5fc5\u8981\u6027\u304c\u5897\u3057\u3066\u304d\u3066\u3044\u307e\u3059\u3002Restek\u306e\u30ab\u30e9\u30e0\u30e9\u30a4\u30f3\u30ca\u30c3\u30d7\u3092\u4ee5\u4e0b\u306e\u8868\u306b\u307e\u3068\u3081\u307e\u3057\u305f\u3002\u5404\u30ab\u30e9\u30e0\u306b\u95a2\u9023\u3059\u308b\u8a18\u4e8b\u3082\u662f\u975e\u3054\u53c2\u7167\u304f\u3060\u3055\u3044\uff01<\/p>\n\n\n

Figure 10:<\/strong> \u70ad\u7d20\u9396\u9577\u3067\u9078\u3076PFAS\u5206\u6790\u306b\u9069\u3057\u305f\u30ab\u30e9\u30e0<\/strong>\u00a0<\/div>
\n\n
\u5206\u6790\u5bfe\u8c61\u306e\u70ad\u7d20\u9396\u9577<\/strong><\/th>\u5206\u6790\u30ab\u30e9\u30e0<\/strong><\/th>\u30c7\u30a3\u30ec\u30a4\u30ab\u30e9\u30e0<\/strong><\/th>\u7279\u9577<\/strong><\/th>\u5185\u5bb9<\/strong><\/th><\/tr><\/thead>
C1\uff5eC14<\/strong> \u8d85\u77ed\u9396\uff5e\u9577\u9396<\/td>Ultra IBD<\/strong> Inert <\/strong>(cat. # 9175312-T<\/a>)<\/td>\u2460TFA\u6e2c\u5b9a\u3057\u306a\u3044: \u30c7\u30a3\u30ec\u30a4\u30ab\u30e9\u30e0\uff0f\u30d5\u30eb\u30dd\u30fc\u30e9\u30b9C18\uff08cat.# 27854<\/a>\uff09
\u2461TFA\u6e2c\u5b9a\u3059\u308b: Ultra IBD\uff08cat.# 9175362<\/a>\uff09<\/td>		\u25cf \u72ec\u81ea\u306e\u6975\u6027\u5b98\u80fd\u57fa\u3092\u57cb\u3081\u8fbc\u3093\u3060\u69cb\u9020
\u25cf \u5f37\u5869\u57fa\u306b\u3082\u512a\u308c\u305f\u30d4\u30fc\u30af\u5206\u96e2
\u25cf \u5e45\u5e83\u3044\u7bc4\u56f2\u3067\u5b89\u5b9a\u3057\u305f\u6027\u80fd\u767a\u63ee<\/td>		\u21d2 \u6975\u6027\u5316\u5408\u7269\u306b\u5bfe\u3059\u308b\u9ad8\u3044\u4fdd\u6301\u529b\u3068\u9078\u629e\u6027\u306b\u3088\u308a\u3001\u591a\u69d8\u306a\u9178\u6027\u6210\u5206\u3092\u9ad8\u611f\u5ea6\u304b\u3064\u52b9\u7387\u7684\u306b\u5206\u6790
\u21d2 \u9006\u76f8\u304a\u3088\u3073HILIC\u6761\u4ef6\u4e0b\u3067\u306e\u6975\u6027\u304a\u3088\u3073\u30a4\u30aa\u30f3\u6027\u5316\u5408\u7269\u306e\u4fdd\u6301\u3082\u53ef\u80fd
\u21d2 pH 2.5\uff5e8\u3001\u6700\u592780\u2103\u306e\u72b6\u6cc1\u4e0b\u3067\u3082\u6d3b\u6027\u30b5\u30a4\u30c8\u3092\u6700\u5c0f\u9650\u306b\u6291\u3048\u305f\u9ad8\u5bc6\u5ea6\u7d50\u5408\u3001\u9ad8\u8010\u4e45\u6027\u3092\u7dad\u6301<\/td><\/tr>
C1\uff5eC4<\/strong> \u8d85\u77ed\u9396\uff5e\u77ed\u9396<\/td>Raptor Polar X<\/strong> (cat. # 9311A52<\/a>)<\/td>\u306a\u3057
\u30a4\u30bd\u30af\u30e9\u30c6\u30a3\u30c3\u30af\u6eb6\u96e2<\/td>		\u25cf \u591a\u69d8\u306a\u6975\u6027\u6210\u5206\u3092\u5206\u96e2
\u25cf \u7c21\u5358\u306a\u30e2\u30fc\u30c9\u5207\u308a\u66ff\u3048
\u25cf MS\u5bfe\u5fdc\u3067\u306e\u9ad8\u901f\/\u9ad8\u611f\u5ea6\u306a\u5206\u6790<\/td>		\u21d2 HILIC\u3068\u30a4\u30aa\u30f3\u4ea4\u63db\u306e2\u3064\u306e\u4fdd\u6301\u30e2\u30fc\u30c9\u3092\u5358\u4e00\u30ea\u30ac\u30f3\u30c9\u306b\u878d\u5408\u3001\u9178\u6027\u3084\u5869\u57fa\u6027\u3001\u7121\u6975\u6027\u3092\u542b\u3080\u5e45\u5e83\u3044\u5206\u6790\u306b\u5bfe\u5fdc
\u21d2 \u7c21\u5358\u306bHILIC\/\u30a4\u30aa\u30f3\u4ea4\u63db\u30e2\u30fc\u30c9\u306e\u5207\u66ff\u3048\u304c\u53ef\u80fd\u3002\u5206\u6790\u6642\u9593\u77ed\u7e2e\u3084\u7c21\u4fbf\u306a\u6761\u4ef6\u5909\u66f4\u306b\u3088\u308a\u4f5c\u696d\u52b9\u7387\u304c\u5411\u4e0a
\u21d2 2.7 \u03bcm\u30b3\u30a2\u30b7\u30a7\u30eb\u7c92\u5b50\u63a1\u7528\u3067\u9ad8\u901f\u5206\u96e2\u3092\u5b9f\u73fe\u3002LC-MS\/MS\u306b\u5bfe\u5fdc\u3057\u3001\u9ad8\u611f\u5ea6\u30fb\u9ad8\u9078\u629e\u6027\u5206\u6790\u306b\u6700\u9069<\/td><\/tr>
C4\u4ee5\u4e0a<\/strong> \u77ed\u9396\uff5e\u9577\u9396<\/td>Force C18<\/strong> (\u30d5\u30eb\u30dd\u30fc\u30e9\u30b9\u30bf\u30a4\u30d7)<\/td>\u30c7\u30a3\u30ec\u30a4\u30ab\u30e9\u30e0\uff0f\u30d5\u30eb\u30dd\u30fc\u30e9\u30b9C18 \uff08cat.# 27854<\/a>\uff09<\/td>\u25cf pH 2\uff5e8\u306e\u7bc4\u56f2\u3067\u5b89\u5b9a\u3057\u305f\u9006\u76f8\u30af\u30ed\u30de\u30c8\u30b0\u30e9\u30d5\u30a3\u30fc
\u25cf \u9ad8\u3044\u70ad\u7d20\u542b\u6709\u91cf\uff0820%\uff09\u306e\u56fa\u5b9a\u76f8
\u25cf 1.8\uff5e5 \u03bcm\u306e\u9ad8\u54c1\u8cea\u591a\u5b54\u6027\u7c92\u5b50<\/td>		\u21d2 \u591a\u69d8\u306a\u30a2\u30d7\u30ea\u30b1\u30fc\u30b7\u30e7\u30f3\u3084\u30de\u30c8\u30ea\u30c3\u30af\u30b9\u306b\u5bfe\u5fdc\u3057\u3001\u512a\u308c\u305f\u30c7\u30fc\u30bf\u54c1\u8cea\u3092\u5b9f\u73fe
\u21d2 \u5f37\u3044\u758e\u6c34\u6027\u4fdd\u6301\u529b\u3092\u767a\u63ee\u3002\u758e\u6c34\u6027\u76f8\u4e92\u4f5c\u7528\u3092\u5229\u7528\u3057\u305f\u5206\u96e2\u306b\u6700\u9069\u3001\u6c4e\u7528\u6027\u306e\u9ad8\u3044\u30af\u30ed\u30de\u30c8\u30b0\u30e9\u30d5\u30a3\u30fc\u5206\u6790\u304c\u53ef\u80fd
\u21d2 HPLC\u304b\u3089UHPLC\u3078\u306e\u79fb\u884c\u3082\u30b9\u30e0\u30fc\u30ba\u3067\u3001MAX1,034 bar\u306e\u8010\u5727\u6027\u80fd\u3001\u9577\u671f\u306e\u5b89\u5b9a\u7a3c\u50cd\u3001\u30ed\u30c3\u30c8\u9593\u518d\u73fe\u6027\u3092\u4fdd\u8a3c<\/td><\/tr>
C6\u4ee5\u4e0a<\/strong> PFOA, PFOS, PFHxS\u306a\u3069<\/td>Raptor C18<\/strong> (\u30b3\u30a2\u30b7\u30a7\u30eb\u30bf\u30a4\u30d7)<\/td>\u30c7\u30a3\u30ec\u30a4\u30ab\u30e9\u30e0\uff0f\u30d5\u30eb\u30dd\u30fc\u30e9\u30b9C18 \uff08cat.# 27854<\/a>\uff09<\/td>\u25cf \u9ad8\u901f\u30fb\u9ad8\u7cbe\u5ea6LC-MS\/MS\u7528\u30ab\u30e9\u30e0
\u25cf 5 \u00b5m SPP\u7c92\u5b50\u3092\u63a1\u7528
\u25cf pH 2\uff5e8\u3067\u4f7f\u7528\u53ef\u80fd<\/td>		\u21d2 \u8868\u9762\u304c\u30b9\u30c6\u30ea\u30c3\u30af\u4fdd\u8b77\u3055\u308c\u305fC18\u56fa\u5b9a\u76f8\u3067\u3001\u5f37\u9178\u6027\u30e2\u30d0\u30a4\u30eb\u30d5\u30a7\u30fc\u30ba\u306b\u3082\u8010\u3048\u5b89\u5b9a\u3057\u305f\u4fdd\u6301\u7279\u6027\u3092\u7dad\u6301
\u21d2 \u5f93\u6765\u306e\u30ab\u30e9\u30e0\u3088\u308a\u9ad8\u901f\u5206\u6790\u304c\u53ef\u80fd\u3002\u8010\u5727\u6027\u80fd\u3082\u9ad8\u304f\u3001\u9023\u7d9a\u4f7f\u7528\u3067\u3082\u518d\u73fe\u6027\u3092\u4fdd\u3064\u305f\u3081\u751f\u7523\u6027\u304c\u5411\u4e0a
\u21d2 \u758e\u6c34\u6027\u5316\u5408\u7269\u3092\u9ad8\u611f\u5ea6\u304b\u3064\u30b7\u30e3\u30fc\u30d7\u306a\u30d4\u30fc\u30af\u3067\u5206\u96e2<\/td><\/tr><\/tbody><\/table><\/figure>\n\n<\/div><\/div><\/div>\n\n\n
<\/div>\n\n\n
Figure 11:<\/strong> \u4e00\u6589\u5206\u6790\u306b\u5bfe\u5fdc\u53ef\u80fd\u306a\u30ab\u30e9\u30e0<\/strong><\/div>
\n\n
\"\"<\/figure>\n\n<\/div><\/div><\/div>\n\n\n
<\/div>\n\n\n\n

\u53c2\u8003\u8a18\u4e8b\uff1a<\/strong>
\u300cPFAS\u5206\u6790\u6cd5\u306e\u9769\u65b0\uff1a\u8d85\u77ed\u9396\uff5e\u9577\u9396PFAS\u3092\u4e00\u6589\u5206\u6790<\/a>\u300d\uff08IBD\u30ab\u30e9\u30e0\u4f7f\u7528\uff09
\u300cRaptor Polar X\uff1a\u591a\u69d8\u306a\u6975\u6027\u6210\u5206\u3092\u5206\u96e2\u3059\u308b\u65b0\u3057\u3044\u30cf\u30a4\u30d6\u30ea\u30c3\u30c9LC\u30ab\u30e9\u30e0<\/a>\u300d
\u300cRaptor C18 SPP 5 \u00b5m \u30ab\u30e9\u30e0\uff1a PFAS\u306e\u8fc5\u901f\u3067\u9ad8\u7cbe\u5ea6\u306aLC-MS\/MS\u306b\u3088\u308b\u5206\u6790\u306b\u6700\u9069\u306a\u9078\u629e\u80a2<\/a>\u300d
\u300cPFAS\u5206\u6790\u306e\u65b0\u6a19\u6e96\uff01Force C18\u30ab\u30e9\u30e0\u3067\u5b9f\u73fe\u3059\u308bPFBA\u5206\u96e2\u3068\u9ad8\u901f\u76f4\u63a5\u6ce8\u5165\u6cd5<\/a>\u300d<\/p>\n\n\n\n

3. PFAS\u7531\u6765\u306e\u30b3\u30f3\u30bf\u30df\u5bfe\u7b56\u306b\u4e0d\u53ef\u6b20\u306a\u30c7\u30a3\u30ec\u30a4\u30ab\u30e9\u30e0\uff08Delay Column\uff09<\/h2>\n\n\n\n

PFAS\u5206\u6790\u306b\u304a\u3044\u3066\u3001\u691c\u51fa\u4e0b\u9650\u304c ng\/L\u30ec\u30d9\u30eb\u3068\u6975\u3081\u3066\u4f4e\u6fc3\u5ea6\u3067\u3042\u308b\u3053\u3068\u304b\u3089\u3001\u5206\u6790\u7cfb\uff08LC-MS\/MS\uff09\u306b\u7531\u6765\u3059\u308b\u30d0\u30c3\u30af\u30b0\u30e9\u30a6\u30f3\u30c9\u6c5a\u67d3\u306e\u5f71\u97ff\u304c\u975e\u5e38\u306b\u9855\u8457\u3068\u306a\u308a\u307e\u3059\u3002\u7279\u306b\u3001LC\u30b7\u30b9\u30c6\u30e0\u306e\u30c1\u30e5\u30fc\u30d6\u3001\u30d0\u30eb\u30d6\u3001\u30b7\u30fc\u30eb\u6750\u3001\u6eb6\u5a92\u5bb9\u5668\u306a\u3069\u304b\u3089\u6eb6\u51fa\u3059\u308bPFAS\u6210\u5206\u304c\u3001\u691c\u51fa\u5bfe\u8c61\u3068\u540c\u4e00\u306e\u4fdd\u6301\u6642\u9593\u306b\u6d41\u51fa\u3059\u308b\u3053\u3068\u3067\u3001\u507d\u967d\u6027\u307e\u305f\u306f\u5b9a\u91cf\u8aa4\u5dee\u306e\u539f\u56e0\u3068\u306a\u308b\u30b1\u30fc\u30b9\u304c\u5c11\u306a\u304f\u3042\u308a\u307e\u305b\u3093\u3002\u3053\u306e\u3088\u3046\u306a\u30b7\u30b9\u30c6\u30e0\u30d6\u30e9\u30f3\u30af\u7531\u6765\u306e\u30b3\u30f3\u30bf\u30df\u30cd\u30fc\u30b7\u30e7\u30f3\u3092\u8b58\u5225\u30fb\u56de\u907f\u3059\u308b\u305f\u3081\u306b\u52b9\u679c\u7684\u306a\u624b\u6bb5\u304c\u3001\u300c\u30c7\u30a3\u30ec\u30a4\u30ab\u30e9\u30e0\uff08Delay Column\uff09\u300d\u306e\u5c0e\u5165\u3067\u3059\u3002\u3053\u3061\u3089\u306e\u8a18\u4e8b\u300c\u30c7\u30a3\u30ec\u30a4\u30ab\u30e9\u30e0\u3092\u7528\u3044\u305f\u30b7\u30b9\u30c6\u30e0\u7531\u6765\u306ePFAS\u306b\u3088\u308b\u59a8\u5bb3\u9664\u53bb<\/a>\u300d\u3082\u3054\u53c2\u7167\u4e0b\u3055\u3044\u3002
\u3010\u30c7\u30a3\u30ec\u30a4\u30ab\u30e9\u30e0\u306e\u5f79\u5272\u3068\u5c0e\u5165\u52b9\u679c\u3011<\/strong><\/p>\n\n\n\n

\u9805\u76ee<\/strong><\/th>\u5185\u5bb9<\/strong><\/th><\/tr><\/thead>
\u4f4d\u7f6e<\/td>\u5206\u6790\u30ab\u30e9\u30e0\u3088\u308a\u524d\u306e\u3001\u30dd\u30f3\u30d7\u3068\u8a66\u6599\u6ce8\u5165\u4f4d\u7f6e\u3068\u306e\u9593\u306b\u8a2d\u7f6e<\/td><\/tr>
\u6a5f\u80fd<\/td>LC\u30b7\u30b9\u30c6\u30e0\u7531\u6765\u306ePFAS\uff08\u7279\u306b PFOA, PFOS \u306a\u3069\uff09\u3092\u5206\u6790\u5bfe\u8c61\u6210\u5206\u3088\u308a\u3082\u5f8c\u306b\u6eb6\u51fa\u3055\u305b\u308b\u3053\u3068\u3067\u3001\u5206\u6790\u30af\u30ed\u30de\u30c8\u30b0\u30e9\u30e0\u304b\u3089\u5e72\u6e09\u3092\u6392\u9664<\/td><\/tr>
\u52b9\u679c<\/td>\u507d\u967d\u6027\u30fb\u30b3\u30f3\u30bf\u30df\u7531\u6765\u30d4\u30fc\u30af\u306e\u5171\u6eb6\u51fa\u304c\u8d77\u3053\u3089\u306a\u3044\u305f\u3081\u3001\u5206\u6790\u306e\u4fe1\u983c\u6027\u304a\u3088\u3073\u518d\u73fe\u6027\u306e\u78ba\u4fdd\u304c\u53ef\u80fd<\/td><\/tr><\/tbody><\/table><\/figure>\n\n\n\n

PFAS\u5206\u6790\uff5c\u30c7\u30a3\u30ec\u30a4\u30ab\u30e9\u30e0, 5 \u00b5m, 50 x 2.1 mm HPLC\u30ab\u30e9\u30e0<\/a>\uff08cat. # 27854\uff09<\/p>\n\n\n\n

\u7279\u9577<\/strong><\/th>\u5185\u5bb9<\/strong><\/th><\/tr><\/thead>
LC\u30b7\u30b9\u30c6\u30e0\u7531\u6765\u30b3\u30f3\u30bf\u30df\u3092\u5f37\u529b\u306b\u30c8\u30e9\u30c3\u30d7<\/td>\u30b7\u30b9\u30c6\u30e0\u7531\u6765\u30b3\u30f3\u30bf\u30df\u306b\u3088\u308b\u5206\u6790\u5e72\u6e09\u3092\u9632\u3050\u3053\u3068\u3067\u3001\u8d85\u5fae\u91cfPFAS\u5206\u6790\u306e\u4fe1\u983c\u6027\u3092\u5927\u5e45\u306b\u5411\u4e0a<\/td><\/tr>
\u6700\u592715,000 psi\uff081,034 bar\uff09\u5bfe\u5fdc\u306e\u30e6\u30cb\u30d0\u30fc\u30b5\u30eb\u8a2d\u8a08<\/td>\u5168HPLC\/UHPLC\u30b7\u30b9\u30c6\u30e0\u304a\u3088\u3073FPP\u3001SPP\u30bf\u30a4\u30d7\u306e\u3042\u3089\u3086\u308b\u5206\u6790\u30ab\u30e9\u30e0\u306b\u4f7f\u7528\u53ef\u80fd<\/td><\/tr>
\u56fa\u5b9a\u76f8\u306e\u7a2e\u985e\u3092\u554f\u308f\u305a\u4f7f\u7528\u53ef\u80fd<\/td>\u9577\u6642\u9593\u306e\u5e73\u8861\u5316\u6761\u4ef6\u4e0b\u3067\u3082\u30d6\u30ec\u30a4\u30af\u30b9\u30eb\u30fc\u304c\u8d77\u3053\u3089\u305a\u3001\u4f7f\u3044\u3084\u3059\u3044\u63a5\u7d9a\u8a2d\u8a08\u3067\u5373\u5ea7\u306b\u53d6\u308a\u4ed8\u3051\u53ef\u80fd<\/td><\/tr><\/tbody><\/table><\/figure>\n\n\n
Figure 12: \u30c7\u30a3\u30ec\u30a4\u30ab\u30e9\u30e0\u306e\u5f79\u5272<\/strong><\/div>
\n\n
\"\"<\/figure>\n\n<\/div><\/div><\/div>\n\n\n
<\/div>\n\n\n\n

4. \u9ad8\u4fe1\u983c\u6027\u306e PFAS \u6a19\u6e96\u7269\u8cea\uff1aCertified Reference Standards\uff08CRMs\uff09<\/h2>\n\n\n\n

PFOS\u30fbPFOA\u306e\u6b63\u78ba\u306a\u5b9a\u91cf\u306b\u306f\u3001\u4fe1\u983c\u6027\u306e\u9ad8\u3044\u6a19\u6e96\u7269\u8cea\u304a\u3088\u3073\u5185\u90e8\u6a19\u6e96\u306e\u4f7f\u7528\u304c\u4e0d\u53ef\u6b20\u3067\u3059\u3002Restek\u3067\u306f\u3001ISO 17034\u304a\u3088\u3073ISO\/IEC 17025\u306b\u6e96\u62e0\u3057\u305f\u8a8d\u8a3c\u6a19\u6e96\u7269\u8cea\uff08CRM\uff09\u3092\u63d0\u4f9b\u3057\u3066\u3044\u307e\u3059\u3002\u4ee5\u4e0b\u306e\u6210\u5206\u6df7\u5408\u54c1\u3092\u542b\u3081\u3001\u591a\u69d8\u306a\u6210\u5206\u306b\u5bfe\u5fdc\u3057\u305f\u5e45\u5e83\u3044\u6a19\u6e96\u7269\u8cea\u3092\u53d6\u308a\u63c3\u3048\u3066\u304a\u308a\u307e\u3059\u3002\u8a73\u7d30\u306f\u300cRestek PFAS\u5206\u6790\u30bd\u30ea\u30e5\u30fc\u30b7\u30e7\u30f3\uff08Advanced Analytical Solutions for PFAS Analysis\uff09<\/a>\u300d\u304b\u3089\u3054\u78ba\u8a8d\u4e0b\u3055\u3044\uff01
 PFAS \u6c34\u9053\u6c34\u8cea\u57fa\u6e96\uff5cPFAS 3\u6210\u5206\u6df7\u5408\u6a19\u6e96\u6db2\uff5cPFOS PFOA PFHxS | \u8a8d\u8a3c\u6a19\u6e96\u7269\u8cea, 10 \u00b5g\/mL, 1mL\/ampul<\/a>\uff08cat. # 30804\uff09
PFAS\uff08\u6709\u6a5f\u30d5\u30c3\u7d20\u5316\u5408\u7269\uff09\u5206\u6790\u7528\u6a19\u6e96\u8a66\u85ac\uff5cPFAS 4\u6210\u5206\u6df7\u5408\uff5cPFOS PFOA PFHxS PFNA\uff5c \u8a8d\u8a3c\u6a19\u6e96\u7269\u8cea, 10 \u00b5g\/mL, 1mL\/ampul<\/a>\uff08cat. # 30805\uff09<\/p>\n\n\n\n

\u7279\u9577<\/strong><\/th>\u5185\u5bb9<\/strong><\/th><\/tr><\/thead>
\u6df7\u5408\u6a19\u6e96\/\u5358\u54c1\u6a19\u6e96<\/td>\u5358\u4e00\u6210\u5206\u307e\u305f\u306f\u591a\u6210\u5206\u6df7\u5408\u54c1\u3068\u3057\u3066\u4f9b\u7d66\u3000\u5fc5\u8981\u306b\u5fdc\u3058\u3066\u67d4\u8edf\u306a\u9078\u5b9a\u304c\u53ef\u80fd<\/td><\/tr>
\u9ad8\u7d14\u5ea6\u3067\u5747\u4e00\u306a\u7d44\u6210<\/td>\u5206\u6790\u7cbe\u5ea6\u3092\u5411\u4e0a\u3055\u305b\u308b\u305f\u3081\u306b\u53b3\u5bc6\u306b\u7ba1\u7406\u3000\u5206\u6790\u30c7\u30fc\u30bf\u306e\u4e00\u8cab\u6027\u3084\u6a19\u6e96\u5316\u304c\u4fc3\u9032\u3055\u308c\u3001\u4fe1\u983c\u6027\u306e\u9ad8\u3044\u7d50\u679c\u306e\u53d6\u5f97\u304c\u53ef\u80fd<\/td><\/tr>
\u9577\u671f\u4fdd\u5b58\u30fb\u5b89\u5b9a\u6027\u691c\u8a3c\u6e08<\/td>\u6fc3\u5ea6\u30fb\u7d14\u5ea6\u30fb\u4fdd\u5b58\u6761\u4ef6\u306b\u95a2\u3059\u308b\u54c1\u8cea\u4fdd\u8a3c\u66f8\u3092\u4ed8\u5c5e<\/td><\/tr><\/tbody><\/table><\/figure>\n\n\n\n

5. \u6280\u8853\u652f\u63f4\u30fb\u30e1\u30bd\u30c3\u30c9\u6587\u732e\u306e\u63d0\u4f9b<\/h2>\n\n\n\n

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